4,4-硫酰双(甲基苯甲酸)合成路线 (共 6 条)
反应条件
1: chromium (VI)-oxide; acetic acid 2: sulfuric acid View Scheme
参考文献
Murahashi; Anzai
Kobunshi Kagaku, 1946 , vol. 3, p. 33,39
Chem.Abstr., 1950 , p. 11106
参考文献
Murahashi; Anzai
Kobunshi Kagaku, 1946 , vol. 3, p. 33,39
Chem.Abstr., 1950 , p. 11106
反应条件
further solvent ratio and reaction times in first step; Product distribution;
参考文献
Brinon, M.C.; Bertorello, M.M. de; Bertorello, H.E.; Luna, L.
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 1 p. 41 - 50
反应条件
further solvent ratio and reaction times in first step; Product distribution;
参考文献
Brinon, M.C.; Bertorello, M.M. de; Bertorello, H.E.; Luna, L.
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 1 p. 41 - 50
反应条件
potassium hydroxide in ethanol Reflux;
参考文献
Gibson, Harry W.; Brumfield, Kimberly K.; Grisle, Roger A.; Hermann, Christine K. F.
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 17 p. 3856 - 3867
反应条件
1: potassium hydroxide / ethanol / Reflux
2: thionyl chloride; N,N-dimethyl-formamide / 24 h / Reflux
View Scheme
参考文献
Gibson, Harry W.; Brumfield, Kimberly K.; Grisle, Roger A.; Hermann, Christine K. F.
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 17 p. 3856 - 3867