2,3-二甲基-2,3-二硝基丁烷合成路线 （共 158 条）
反应条件
Platin-Anode.Electrolysis;
参考文献
Bahner
Industrial and Engineering Chemistry, 1952 , vol. 44, p. 317
反应条件
aluminum amalgam in tetrahydrofuran; water T=-7 - -2°C; 0.75 h;
参考文献
Rajca, Andrzej; Pink, Maren; Mukherjee, Sumit; Rajca, Suchada; Das, Kausik
Tetrahedron, 2007 , vol. 63, # 44 p. 10731 - 10742
反应条件
hydrogenchloride; tin 3 h; Heating;
参考文献
Hirel, Catherine; Vostrikova, Kira E.; Pecaut, Jacques; Ovcharenko, Victor I.; Rey, Paul
Chemistry - A European Journal, 2001 , vol. 7, # 9 p. 2007 - 2014
反应条件
1: 63 percent / Zn; NH4Cl / tetrahydrofuran; H2O / 3 h / 10 °C 2: 43 percent / methanol / 16 h / 20 °C 3: 84 percent / lead dioxide / methanol / 0.33 h / 20 °C View Scheme
参考文献
Wu, Yihui; Bi, Lanrong; Bi, Wei; Li, Zeng; Zhao, Ming; Wang, Chao; Ju, Jingfang; Peng, Shiqi
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 16 p. 5711 - 5720
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Chemische Berichte, , vol. 90, p. 1769,1773
参考文献
Chemische Berichte, , vol. 90, p. 1769,1773
反应条件
nBu4NPF6 in N,N-dimethyl-formamide T=0°C; electrochemical reduction; var. vicinal dinitro compounds; Mechanism;
参考文献
Bowyer, Walter J.; Evans, Dennis H.
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5234 - 5239
反应条件
1.1: 81 percent / Sn; aq. HCl / 3 h / Heating 2.1: 78 percent / aq. H2SO4 / methanol / 1 h / 20 °C / pH 3 - 4 3.1: m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 / 1 h / Ice cooling 3.2: 12 percent / aq. NaIO4 / CH2Cl2 View Scheme
参考文献
Hirel, Catherine; Vostrikova, Kira E.; Pecaut, Jacques; Ovcharenko, Victor I.; Rey, Paul
Chemistry - A European Journal, 2001 , vol. 7, # 9 p. 2007 - 2014
反应条件
1: 81 percent / Sn; aq. HCl / 3 h / Heating 2: 89 percent / diethyl ether / ice cooling View Scheme
参考文献
Hirel, Catherine; Vostrikova, Kira E.; Pecaut, Jacques; Ovcharenko, Victor I.; Rey, Paul
Chemistry - A European Journal, 2001 , vol. 7, # 9 p. 2007 - 2014
反应条件
1: 79 percent / Al/Hg / tetrahydrofuran; H2O / 0.75 h / -7 - -2 °C 2: 96 percent / p-TsOH*H2O / methanol / 48 h / 20 °C 3: 85 percent / NaIO4 / CHCl3; H2O / 0 - 20 °C View Scheme
参考文献
Wu, Yihui; Bi, Lanrong; Bi, Wei; Li, Zeng; Zhao, Ming; Wang, Chao; Ju, Jingfang; Peng, Shiqi
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 16 p. 5711 - 5720
