2,3-二甲基-2,3-二硝基丁烷合成路线 （共 158 条）
反应条件
oxygen; 1,8-diazabicyclo[5.4.0]undec-7-ene; copper dichloride in N,N-dimethyl-formamide T=20°C;
参考文献
Do, Hien-Quang; Tran-Vu, Hung; Daugulis, Olafs
Organometallics, 2012 , vol. 31, # 22 p. 7816 - 7818
反应条件
1: in water 0.5 h; 2: With ammonia; dihydrogen peroxide in water T=85 - 90°C; pH=10; 0.5 h; Reagent/catalystSolventConcentrationTemperaturepH-valueTime;
参考文献
NINGBO INSTITUE OF TECHNOLOGY ZHEJIANG ZHEJIAND; Zhang, Shengjian; Zhao, Yingxian; Zhang, Hong
Patent: US2013/184504 A1, 2013 ;
Location in patent: Paragraph 0053; 0054; 0055; 0056; 0057; 0058; 0067; 0068 ;
反应条件
1: in water 1 h; 2: With dihydrogen peroxide; sodium hydroxide in water T=80°C; 2 h; Reagent/catalystSolventTemperatureConcentrationTimepH-value;
参考文献
NINGBO INSTITUE OF TECHNOLOGY ZHEJIANG ZHEJIAND; Zhang, Shengjian; Zhao, Yingxian; Zhang, Hong
Patent: US2013/184504 A1, 2013 ;
Location in patent: Paragraph 0107; 0108; 0109; 0110; 0111 ;
反应条件
ozone in chloroform-d1 T=-78°C; 0.25 h;
参考文献
Gagnon, Janet L.; Walters, Thomas R.; Zajac, Walter W.; Buzby, John H.
Journal of Organic Chemistry, 1993 , vol. 58, # 24 p. 6712 - 6715
反应条件
in dimethyl sulfoxide T=18 - 20°C; 0.00833333 h;
参考文献
Wade, Peter A.; Dailey, William P.; Carroll, Patrick J.
Journal of the American Chemical Society, 1987 , vol. 109, # 18 p. 5452 - 5456
反应条件
n-Pentyl nitrite; acetic acid 4 h; Heating;
参考文献
Yandovskii, V. N.; Ryabinkin, I. I.; Tselinskii, I. V.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 10 p. 1773 - 1775
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 10 p. 2084 - 2086
反应条件
sodium 2-methyl-2-propanethiolate in N,N-dimethyl-formamide T=25°C; Irradiation;
参考文献
Amrollah-Madjdabadi, Ali; Beugelmans, Rene; Lechevallier, Andre
Tetrahedron Letters, 1987 , vol. 28, # 39 p. 4525 - 4528
反应条件
K(cryp 2.2.2)(1+); potassium tert-butylate in dimethyl sulfoxide T=25°C; 1.5 h; Irradiation; Yield given;
参考文献
Seigle; Hass
Journal of Organic Chemistry, 1940 , vol. 5, p. 103
反应条件
K(cryp 2.2.2)(1+); potassium tert-butylate in dimethyl sulfoxide T=25°C; 1.5 h; Irradiation; Yield given;
参考文献
Russell, Glen A.; Ros, Francisco; Mudryk, Boguslaw
Journal of the American Chemical Society, 1980 , vol. 102, # 25 p. 7601 - 7603
反应条件
1: 2-Nitropropane With tetra(n-butyl)ammonium hydroxide in dichloromethane; water T=20°C; 0.5 h; Inert atmosphere; 2: 6-nitro-N-propyl-2-trichloromethylquinazolin-4-amine in dichloromethane; water T=20°C; 4 h; UV-irradiationInert atmosphere;
参考文献
Maillard-Boyer, Martine; Castera-Ducros, Caroline; Verhaeghe, Pierre; Sifredi, France; Rathelot, Pascal; Vanelle, Patrice
Molecules, 2010 , vol. 15, # 4 p. 2719 - 2729
