1: With hydrazine hydrate in ethanol 1.5 h; Inert atmosphereReflux; 2: With hydrogenchloride in ethanol; water T=90°C; 15 h; Inert atmosphere; 3: With sodium hydroxide in ethanol; water Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 16, # 33 p. 10171 - 10177
1: dimethylamine borane With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2: para-bromobenzonitrile in tetrahydrofuran; hexane T=65°C; 12 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 66, # 6 p. 1999 - 2004
