1-(碘甲基)-3-硝基-苯合成路线 （共 9 条）
反应条件
AgNO2; diethyl ether; benzene
参考文献
Wygaerts; Eeckhout
Natuurw. Tijdschr., 1935 , vol. 17, p. 163,179
反应条件
monomethyldichlorosilane; iron(III) chloride; sodium iodide in acetonitrile
21 h; Heating;
参考文献
Li, Zhifang; Sheng, Chunqi; Yang, Chengjun; Qiu, Huayu
Organic Preparations and Procedures International, 2007 , vol. 39, # 6 p. 608 - 611
反应条件
aluminum(III) hydrogen sulfate; potassium iodide in hexane
3 h; Heating;
参考文献
Tajik, Hassan; Shirini, Farhad; Zolfigol, Mohammad Ali; Samimi, Faeze
Synthetic Communications, 2006 , vol. 36, # 1 p. 91 - 95
反应条件
sodium iodide in acetone
T=20°C; 20 h;
参考文献
Alajarin, Mateo; Orenes, Raul-Angel; Howard, Judith A. K.; Spencer, Elinor C.; Steed, Jonathan W.; Pastor, Aurelia
Chemistry - A European Journal, 2012 , vol. 18, # 8 p. 2389 - 2397
反应条件
1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione in 1,2-dichloro-ethane
7 h; RefluxFluorescent lighting; Product distribution / selectivity;
参考文献
TECHNION RandD FOUNDATION LTD.; NISNEVICH, Gennady; GANDELMAN, Mark; KULBITSKI, Kseniya
Patent: WO2011/154953 A1, 2011 ;
Location in patent: Page/Page column 28-29 ;
反应条件
tetra-(n-butyl)ammonium iodide; [bmim][InCl4]
T=135 - 140°C; 0.05 h; Microwave irradiationNeat (no solvent); chemoselective reaction;
参考文献
Mirjafari, Arsalan; Mohammadpoor-Baltork, Iraj; Moghadam, Majid; Tangestaninejad, Shahram; Mirkhani, Valiollah; Khosropour, Ahmad Reza
Tetrahedron Letters, 2010 , vol. 51, # 25 p. 3274 - 3276
反应条件
tetra-(n-butyl)ammonium iodide; [bmim][InCl4]
T=135 - 140°C; 0.05 h; Microwave irradiationNeat (no solvent); chemoselective reaction;
参考文献
Mirjafari, Arsalan; Mohammadpoor-Baltork, Iraj; Moghadam, Majid; Tangestaninejad, Shahram; Mirkhani, Valiollah; Khosropour, Ahmad Reza
Tetrahedron Letters, 2010 , vol. 51, # 25 p. 3274 - 3276
反应条件
sodium iodide in acetone
0.333333 h;
参考文献
Zhou; Wang; Chang; Chen; Cheng; Lee
Journal of Medicinal Chemistry, 1991 , vol. 34, # 12 p. 3346 - 3350
反应条件
chloro-trimethyl-silane; 1,1,3,3-tetramethyldisiloxane; sodium iodide
1.) acetonitrile, room temperature, 10 min, 2.) 30 min, 80 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Aizpurua, Jesus M.; Palomo, Claudio
Tetrahedron Letters, 1984 , vol. 25, # 10 p. 1103 - 1104
