2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖合成路线 (共 199 条)
反应条件
water; silver carbonate in acetone 0.5 h;
参考文献
Sabesan; Neira
Carbohydrate Research, 1992 , vol. 223, p. 169 - 185
反应条件
hydrazinium monoacetate in N,N-dimethyl-formamide T=60°C; 0.666667 h;
参考文献
Das, Saibal Kumar; Reddy, K. Anantha; Mukkanti
Carbohydrate Research, 2007 , vol. 342, # 15 p. 2309 - 2315
反应条件
hydrazinium monoacetate in N,N-dimethyl-formamide T=55°C; Deacetylation; 0.25 h;
参考文献
Ren, Tan; Dexi, Liu
Tetrahedron Letters, 1999 , vol. 40, # 43 p. 7621 - 7625
反应条件
triethylamine; aminomethylated polystyrene resin in tetrahydrofuran T=75°C; 18 h;
参考文献
Johnsson, Richard; Ellervik, Ulf
Synlett, 2005 , # 19 art. no. D29405ST, p. 2939 - 2940
反应条件
trichloroisocyanuric acid; water in acetone T=0 - 20°C; 0.5 h; Green chemistry; Reagent/catalystSolvent;
参考文献
Basu, Nabamita; Maity, Sajal Kumar; Chaudhury, Aritra; Ghosh, Rina
Carbohydrate Research, 2013 , vol. 369, p. 10 - 13
反应条件
AcrH(+)I(-); sodium cyanoborohydride in acetonitrile T=20°C; 240 h;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
NISacc in water; acetonitrile T=20°C; 0.0833333 h;
参考文献
Mandal, Pintu Kumar; Misra, Anup Kumar
Synlett, 2007 , # 8 p. 1207 - 1210
反应条件
NISacc in water; acetonitrile T=20°C; 0.333333 h;
参考文献
Mandal, Pintu Kumar; Misra, Anup Kumar
Synlett, 2007 , # 8 p. 1207 - 1210
反应条件
sodium cyanoborohydride in nitromethane T=100°C; 10.5 h; Inert atmosphere;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
N,N,N',N'-tetramethyl-urea; silver trifluoromethanesulfonate in various solvent(s) T=25°C; 1.5 h; Yields of byproduct given;
参考文献
Takeo, Ken'ichi
Carbohydrate Research, 1980 , vol. 87, p. 147 - 152