potassium fluoride; C114H158O4P2Pd2; silver fluoride in tert-butyl methyl ether T=110°C; 14 h; Sealed tube;

暂无反应条件数据

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 14 h / 0 - 20 °C 2.1: tetrabutylammomium bromide / dichloromethane / 0.17 h / 20 °C / |Inert atmosphere; |Molecular sieve 2.2: 20 °C / |Inert atmosphere View Scheme

1.1: sulfuric acid / acetone / 2 h / 0 - 10 °C / Inert atmosphere; Large scale reaction 2.1: sulfur trioxide / 19 h / 30 °C / Inert atmosphere; Large scale reaction 2.2: 7 h / 30 - 70 °C / Inert atmosphere View Scheme

sulfuric acid in acetone T=0 - 10°C; 2 h; Inert atmosphereLarge scale reaction;