2,4,4-三甲基己二酸合成路线 (共 18 条)
反应条件
1: Ba(OH)2, MnCO3 / 250 - 255 °C 2: (i), (ii) Al2O3, (heating), (iii) H2, Ni View Scheme
参考文献
Slomp,G. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 514 - 518
反应条件
barium dihydroxide; manganese dihydrogen carbonate T=250 - 255°C;
参考文献
Qudrat-i-Khuda; Mukherji
Journal of the Indian Chemical Society, 1946 , vol. 23, p. 435,439
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Birch; Johnson
Journal of the Chemical Society, 1951 , p. 1493,1495
反应条件
potassium permanganate in acetone
参考文献
Cavill,G.W.K.; Solomon,D.H.
Australian Journal of Chemistry, 1962 , vol. 15, p. 764 - 770
反应条件
1: Na / butan-1-ol
2: KMnO4 / acetone
View Scheme
参考文献
Cavill,G.W.K.; Solomon,D.H.
Australian Journal of Chemistry, 1962 , vol. 15, p. 764 - 770
反应条件
sodium hydroxide; dihydrogen peroxide; magnesium sulfate
参考文献
Payne
Journal of Organic Chemistry, 1959 , vol. 24, p. 719
反应条件
sodium hydroxide; potassium permanganate
参考文献
Mazur,R.H.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1289 - 1291
反应条件
1: aqueous HCl
2: aqueous NaOH-solution; aqueous hydrogen peroxide; magnesium sulfate
View Scheme
参考文献
Payne
Journal of Organic Chemistry, 1959 , vol. 24, p. 719
反应条件
1: methanol; aqueous hydrogen peroxide; aq. NaOH solution
2: aqueous HCl
3: aqueous NaOH-solution; aqueous hydrogen peroxide; magnesium sulfate
View Scheme
参考文献
Payne
Journal of Organic Chemistry, 1959 , vol. 24, p. 719
反应条件
1: toluene-4-sulfonic acid
2: (i) aq. H2O2, HCO2H, (ii) aq. NaMnO4
View Scheme
参考文献
Slomp,G. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 514 - 518
反应条件
1: aq. HBr
2: aq. NaOH, KMnO4
View Scheme
参考文献
Mazur,R.H.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1289 - 1291