4-甲氧基苯-1,2-二醇合成路线 （共 26 条）
反应条件
oxalic acid in water
参考文献
Jurd,L. et al.
Phytochemistry (Elsevier), 1972 , vol. 11, p. 3287 - 3292
反应条件
1: aq. H2O2, NaOH 2: 3,4,5,6-tetrachloro-<1,2>benzoquinone / dioxane 3: (i) TsNHNH2, CH2Cl2, (ii) Al2O3 4: H3PO2, aq. HCl / ethanol 5: aq. NaOH / Heating View Scheme
参考文献
Horner,L.; Weber,K.-H.
Chemische Berichte, 1963 , vol. 96, p. 1568 - 1578
反应条件
sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; water
T=20°C; Dakin reaction; 1 h;
参考文献
Bernet, Andreas; Seifert, Karlheinz
Helvetica Chimica Acta, 2006 , vol. 89, # 4 p. 784 - 796
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in ethanol
T=40°C; 19 h;
参考文献
Aihara, Kazuhiro; Urano, Yasuteru; Higuchi, Tsunehiko; Hirobe, Masaaki
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 11 p. 2165 - 2170
反应条件
water; oxygen; copper; Cu2Cl2
1.) CH3CN; Multistep reaction;
参考文献
Capdevielle, Patrice; Maumy, Michel
Tetrahedron Letters, 1982 , vol. 23, # 15 p. 1577 - 1580
反应条件
NADH-H+ in water; acetonitrile
T=30°C; pH=7.0; Rate constant;
参考文献
Carlson, Brian W.; Miller, Larry L.
Journal of the American Chemical Society, 1985 , vol. 107, # 2 p. 479 - 485
反应条件
1: 75 percent / boric acid; aq. H2O2; aq. H2SO4 / tetrahydrofuran / 12 h / 20 °C
2: 67 percent / potassium carbonate / acetone / 6 h / Heating
3: 77 percent / H2 / Pd/C / atmospheric pressure
View Scheme
参考文献
Saito, Shizuka; Kawabata, Jun
Tetrahedron, 2005 , vol. 61, # 34 p. 8101 - 8108
反应条件
1: 67 percent / potassium carbonate / acetone / 6 h / Heating
2: 77 percent / H2 / Pd/C / atmospheric pressure
View Scheme
参考文献
Saito, Shizuka; Kawabata, Jun
Tetrahedron, 2005 , vol. 61, # 34 p. 8101 - 8108
反应条件
1: 84 percent / potassium carbonate / acetone / 4 h / Heating
2: 75 percent / boric acid; aq. H2O2; aq. H2SO4 / tetrahydrofuran / 12 h / 20 °C
3: 67 percent / potassium carbonate / acetone / 6 h / Heating
4: 77 percent / H2 / Pd/C / atmospheric pressure
View Scheme
参考文献
Saito, Shizuka; Kawabata, Jun
Tetrahedron, 2005 , vol. 61, # 34 p. 8101 - 8108
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Kvalnes
Journal of the American Chemical Society, 1934 , vol. 56, p. 2487
Full Text View citing articles Show Details
Rosenblatt; Rosenthal
Journal of the American Chemical Society, 1953 , vol. 75, p. 4607
