3-苄磺酰基-1H-1,2,4-噻唑-5-胺合成路线 （共 14 条）
反应条件
sodium hydroxide in ethanol
参考文献
Schering Agrochemicals
Patent: US4889553 A1, 1989 ;
反应条件
sodium hydroxide in ethanol
参考文献
Schering Agrochemicals
Patent: US4889553 A1, 1989 ;
反应条件
sodium hydroxide in ethanol; water T=20 - 25°C; 4 h;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2004/46149 A1, 2004 ;
Location in patent: Page/Page column 28 ;
反应条件
in water; N,N-dimethyl-formamide
参考文献
Tolstyakov; Pevzner; Tselinskii
Russian Journal of General Chemistry, 2000 , vol. 70, # 9 p. 1458 - 1465
反应条件
sodium hydride
1) toluene, DMF, 0 deg C, 0.5 h, 2) 0 deg C, 3 h, r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Reiter, J.; Somorai, T.; Dvortsak, P.; Bujtas, Gy.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 385 - 394
反应条件
sodium hydride
1) toluene, DMF, 0 deg C, 0.5 h, 2) 0 deg C, 3 h, r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Reiter, J.; Somorai, T.; Dvortsak, P.; Bujtas, Gy.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 385 - 394
反应条件
sodium methylate in methanol; ethanol; water
参考文献
THE DOW CHEMICAL COMPANY
Patent: EP142152 B1, 1991 ;
反应条件
1: With sodium methylate in methanol; ethanol
120 h; Reflux;
2: With hydrogenchloride; water
参考文献
Chen, Chao-Nan; Lv, Li-Li; Ji, Feng-Qin; Chen, Qiong; Xu, Hui; Niu, Cong-Wei; Xi, Zhen; Yang, Guang-Fu
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 8 p. 3011 - 3017
反应条件
1.) NaOPr
1.) n-PrOH, 5 min, 2.) n-PrOH, from 104 to 108 deg C, 5 h; Yield given. Multistep reaction;
参考文献
McKendry
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 3 p. 231 - 240
反应条件
sodium methylate in methanol
96 h; Heating;
参考文献
Monte, William T.; Kleschick, William A.; Bordner, Jon
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 1 p. 183 - 188
