4-氟-2,6-二甲基苯胺合成路线 （共 10 条）
反应条件
palladium 10 on activated carbon; hydrogen in acetic acid P=3750.38 Torr; 5 h;
参考文献
Leuthaeusser, Steffen; Schmidts, Volker; Thiele, Christina M.; Plento, Herbert
Chemistry - A European Journal, 2008 , vol. 14, # 18 p. 5465 - 5481
反应条件
1: (i) PCl5, (ii) aq. NH3 2: aq. NaOH, Br2 3: (i) aq. HCl, NaNO2, (ii) HPF6 4: H2 / Pd-C View Scheme
参考文献
Dewar,M.J.S.; Takeuchi,Y.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 390 - 394
反应条件
1: (i) aq. HCl, NaNO2, (ii) HPF6 2: H2 / Pd-C View Scheme
参考文献
Dewar,M.J.S.; Takeuchi,Y.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 390 - 394
反应条件
1: aq. NaOH, Br2 2: (i) aq. HCl, NaNO2, (ii) HPF6 3: H2 / Pd-C View Scheme
参考文献
Dewar,M.J.S.; Takeuchi,Y.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 390 - 394
反应条件
1: acetic acid anhydride; acetic acid; nitric acid 2: Raney nickel; ethanol / Hydrogenation View Scheme
参考文献
Valkanas,G.
Journal of the Chemical Society, 1963 , p. 5554 - 5556
反应条件
sulfuric acid; sodium nitrite
参考文献
Dewar,M.J.S.; Takeuchi,Y.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 390 - 394
反应条件
(i) NaNO2, aq. HCl, (ii) /BRN= 4652394/; Multistep reaction;
参考文献
Dewar,M.J.S.; Takeuchi,Y.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 390 - 394
反应条件
1.) diazotization, 2.) Sandmeyer reaction; Yield given. Multistep reaction;
参考文献
Dell'Erba, Carlo; Sancassan, Fernando; Novi, Marino; Petrillo, Giovanni; Mugnoli, Angelo; et al.
Journal of Organic Chemistry, 1988 , vol. 53, # 15 p. 3564 - 3568
反应条件
1: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/ 2: (i) H2SO4, (ii) H2O 3: H3PO4 / 150 °C View Scheme
参考文献
Dewar,M.J.S.; Takeuchi,Y.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 390 - 394
反应条件
(i) aq. HCl, NaNO2, (ii) CuCl, aq. HCl; Multistep reaction;
参考文献
Dewar,M.J.S.; Takeuchi,Y.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 390 - 394
