二(3-甲氧基苯基)甲酮合成路线 （共 15 条）
反应条件
pyridinium chlorochromate in dichloromethane
参考文献
Dharanipragada, Ramalinga; Ferguson, Stephen B.; Diederich, Francois
Journal of the American Chemical Society, 1988 , vol. 110, # 6 p. 1679 - 1690
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); di-tert-butyl peroxide; 1,2-bis-(diphenylphosphino)ethane in benzene
T=160°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Yang, Luo; Zeng, Tieqiang; Shuai, Qi; Guo, Xiangyu; Li, Chao-Jun
Chemical Communications, 2011 , vol. 47, # 7 p. 2161 - 2163
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=80°C; 4 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Venkatesh, Varadhachari; Dasgupta, Priyabrata
Tetrahedron Letters, 2010 , vol. 51, # 38 p. 4975 - 4980
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=60°C; 4 h;
参考文献
Rao, Maddali L. N.; Venkatesh, Varadhachari; Dasgupta, Priyabrata
Tetrahedron Letters, 2010 , vol. 51, # 38 p. 4975 - 4980
反应条件
potassium phosphate; oxygen; copper diacetate; p-toluidine; sodium sulfate in dimethyl sulfoxide
T=140°C; 6 h; Sealed tube;
参考文献
Maji, Arun; Rana, Sujoy; Akanksha; Maiti, Debabrata
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2428 - 2432
Angew. Chem., 2014 , vol. 126, # 9 p. 2460 - 2464,5
参考文献
Klemm et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 349,352
反应条件
1: 62 percent / magnesium / diethyl ether / 1 h / Ambient temperature
2: 90 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / 20 °C
View Scheme
参考文献
Dharanipragada, Ramalinga; Ferguson, Stephen B.; Diederich, Francois
Journal of the American Chemical Society, 1988 , vol. 110, # 6 p. 1679 - 1690
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=80°C; 4 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Venkatesh, Varadhachari; Dasgupta, Priyabrata
Tetrahedron Letters, 2010 , vol. 51, # 38 p. 4975 - 4980
反应条件
bis(1,5-cyclooctadiene)nickel (0) in N,N-dimethyl-formamide
15 h; Ambient temperature;
参考文献
Goto, Toshio; Onaka, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 1980 , p. 51 - 52
参考文献
Celgene Corporation
Patent: US2005/107339 A1, 2005 ;
