4-(1,4-二甲基-1-乙基)戊基酚合成路线 （共 26 条）
反应条件
1: 52 percent / t-BuOK / tetrahydrofuran / 1 h / Heating 2: 100 percent / AsPh3 / Pd2dba3*CHCl3 / dimethylformamide / 2 h / 20 °C View Scheme
参考文献
Wada, Akimori; Ieki, Yasuhiro; Ito, Masayoshi
Synlett, 2002 , # 7 p. 1061 - 1064
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 0.5 h;
参考文献
Neill, Steven J.; Horgan, Roger
Phytochemistry (Elsevier), 1983 , vol. 22, # 11 p. 2469 - 2472
反应条件
1.1: NaNH2 / diethyl ether / 0.75 h 1.2: 87 percent / diethyl ether / 0.75 h 2.1: tBuOK; BuLi / hexane / 1 h / 25 °C 2.2: 54 percent / fluorodimethoxyborane diethyl etherate; H2O2 (30percent); NaOH (3.0 M) / hexane / 1 h / 25 °C View Scheme
参考文献
Rauchschwalbe, Guenter; Zellner, Armin; Schlosser, Manfred
European Journal of Organic Chemistry, 2001 , # 20 p. 3903 - 3909
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Matsui et al.
Journal of Vitaminology, 1958 , vol. 4, p. 190,192
Full Text Show Details
N. V. Philips' Gloeilampenfabr.
Patent: GB751753 , 1953 ;
Full Text Show Details
Huisman et al.
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 899,911
Recueil des Travaux Chimiques des Pays-Bas, 1956 , vol. 75, p. 977,1003
反应条件
1: 85 percent / 0 °C 2: 90 percent / DibAl-H / -78 °C View Scheme
参考文献
Vuligonda, Vidyasagar; Garst, Michael E.; Chandraratna, Roshantha A.S.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 4 p. 589 - 594
参考文献
Sopher, David W.; Utley, James H. P.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 8 p. 1361 - 1368
反应条件
1: ethanolic NaOH-solution 2: LiAlH4; diethyl ether View Scheme
参考文献
Huisman et al.
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 899,911
Recueil des Travaux Chimiques des Pays-Bas, 1956 , vol. 75, p. 977,1003
反应条件
1: pyridine / Behandeln des Reaktionsprodukts mit methanol. Kalilauge 2: ethanolic NaOH-solution 3: LiAlH4; diethyl ether View Scheme
参考文献
Huisman et al.
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 899,911
Recueil des Travaux Chimiques des Pays-Bas, 1956 , vol. 75, p. 977,1003
反应条件
1: petroleum ether; MnO2 / <30 2: KOH 3: 2,4-dimethyl-pyridine; copper (II)-acetate View Scheme
参考文献
Salman, Mohammad; Babu, Suresh J.; Kaul, Vijay K.; Ray, Purna C.; Kumar, Naresh
Organic Process Research and Development, 2005 , vol. 9, # 3 p. 302 - 305
反应条件
tributylphosphine; phenyl isocyanate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile 5 h; Heating;
参考文献
Okukado, Nobuhisa; Uchikawa, Osamu; Nakamura, Yukari
Chemistry Letters, 1988 , # 8 p. 1449 - 1452
