1-(4-甲氧基苯基)-2-(4-硝基苯基)-乙炔合成路线 （共 24 条）
反应条件
N-iodo-succinimide; trimethylsilylazide in 1,2-dichloro-ethane; acetonitrile T=20 - 70°C; 3 h;
参考文献
Organic Letters, , vol. 15, # 11 p. 2571 - 2573
反应条件
N-iodo-succinimide; trimethylsilylazide in 1,2-dichloro-ethane; acetonitrile T=20 - 70°C; 3 h;
参考文献
Organic Letters, , vol. 15, # 11 p. 2571 - 2573
反应条件
Ph2P(CH2CH2O)22CH3; triethylamine; palladium dichloride in water
T=80°C; Sonogashira coupling; 3 h; Inert atmosphere;
参考文献
Liu, Ning; Liu, Chun; Xu, Qiang; Jin, Zilin
European Journal of Organic Chemistry, 2011 , # 23 p. 4422 - 4428
反应条件
KOC(O)Ph; triphenylphosphine; copper(l) chloride in 1,3-dimethyl-imidazolidin-2-one
T=120°C; Sila-Sonogashira-Hagihara cross-coupling reaction; 12 h; Inert atmosphere;
参考文献
Ihara, Hideki; Ueda, Akinori; Suginome, Michinori
Chemistry Letters, 2011 , vol. 40, # 9 p. 972 - 974
反应条件
1: para-iodoanisole; trimethylsilylacetylene With potassium carbonate in methanol; acetonitrile
T=40°C; Sonogashira Cross-Coupling; 2 h;
2: para-nitro iodo-benzene in methanol; acetonitrile
T=40°C; Sonogashira Cross-Coupling; 2 h; chemoselective reaction;
参考文献
Mandali, Pavan Kumar; Chand, Dillip Kumar
Catalysis Communications, 2014 , vol. 47, p. 40 - 44
反应条件
silver fluoride; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0) in acetonitrile
T=20°C; Hiyama Coupling; 12 h;
参考文献
Tang, Jiansheng; Guo, Cancheng
Journal of Chemical Research, 2014 , vol. 38, # 2 p. 123 - 127
反应条件
K3PO4*3H2O in methanol
T=80°C; Sonogashira coupling; 3 h; Inert atmosphere;
参考文献
Lin, Cai-Xia; Zhu, Jia-Fang; Li, Qing-Shan; Ao, Li-Hua; Jin, Yan-Juan; Xu, Feng-Bo; Hu, Fang-Zhong; Yuan, Yao-Feng
Applied Organometallic Chemistry, 2014 , vol. 28, # 4 p. 298 - 303
反应条件
bis-triphenylphosphine-palladium(II) chloride; ammonium hydroxide; copper(l) iodide in tetrahydrofuran
T=20°C; Sonogashira coupling; 8 h;
参考文献
Mori, Atsunori; Mohamed Ahmed, Mohamed S.; Sekiguchi, Akitoshi; Masui, Kentaro; Koike, Tooru
Chemistry Letters, 2002 , # 7 p. 756 - 757
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=90°C; 2 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
Organic Letters, 2010 , vol. 12, # 9 p. 2048 - 2051
反应条件
water; potassium carbonate; 1,3-diphenyl-1,3-propanedione; copper(I) bromide in N,N-dimethyl-formamide
T=120°C; 20 h; Sealed tubeIn air;
参考文献
Pan, Delin; Zhang, Chun; Ding, Shengtao; Jiao, Ning
European Journal of Organic Chemistry, 2011 , # 25 p. 4751 - 4755
