反应条件
LDA in tetrahydrofuran; hexane (inert atmosphere); addn. of LDA in THF/hexane at -78°C to the cyclopropene in THF, stirring (-30°C, 1 h), addn. of Me3GeCl, stirring (room temp., 15 h), quenching with satd. aq. NH4Cl; filtration, phase sepn., washing (H2O), drying (MgSO4), concn. (rotavapor), gas chromy.;
参考文献
Eckert-Maksic, Mirjana; Elbel, Susanne; Stohlmeier, Michael; Untiedt, Sven; De Meijere, Armin
Chemische Berichte, 1996 , vol. 129, # 2 p. 169 - 174
