6-甲氧基-2-乙酰萘合成路线 （共 124 条）
反应条件
mercury(II) fluoride; oxygen in acetonitrile T=25°C; 24 h; Irradiation;
参考文献
Farhadi, Saeid; Zaringhadam, Parisa; Sahamieh, Reza Zarei
Tetrahedron Letters, 2006 , vol. 47, # 12 p. 1965 - 1968
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; Candida antarctica B lipase; [RuCl2(p-cymene)]2; (E)-2-((1-hydroxy-2-methylpropan-2-ylimino)methyl)phenol in toluene T=70°C; 72 h; Inert atmosphereEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Merabet-Khelassi, Mounia; Vriamont, Nicolas; Aribi-Zouioueche, Louisa; Riant, Olivier
Tetrahedron Asymmetry, 2011 , vol. 22, # 18-19 p. 1790 - 1796
反应条件
in nitrobenzene (acetylation);
参考文献
Pivsa-Art, Sommai; Okuro, Kazumi; Miura, Masahiro; Murata, Satoru; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 13 p. 1703 - 1708
反应条件
antimony(III) trifluorosulphonate; lithium perchlorate in nitromethane T=50°C; Acetylation; Friedel-Crafts acylation; 5 h;
参考文献
Kobayashi; Komoto
Tetrahedron, 2000 , vol. 56, # 35 p. 6463 - 6465
反应条件
1: With N-iodo-succinimide; N-hexadecyl-N,N,N-trimethylammonium bromide in 1,4-dioxane; water T=115°C; 0.25 h; Microwave irradiation; 2: With dipyridinium dichromate; acetic acid in 1,4-dioxane; water T=115°C; 0.25 h; Microwave irradiation;
参考文献
Sharma, Naina; Sharma, Abhishek; Kumar, Rakesh; Shard, Amit; Sinha, Arun K.
European Journal of Organic Chemistry, 2010 , # 31 p. 6025 - 6032
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; Pd((-)-sparteine)2Cl2 in tert-butyl alcohol T=65°C; 20 h;
参考文献
Nagaoka, Hiroyuki
ACS Catalysis, 2014 , vol. 4, # 2 p. 553 - 565
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78 - -70°C; 1.5 h;
参考文献
Matsunaga, Nobuyuki; Kaku, Tomohiro; Ojida, Akio; Tanaka, Toshimasa; Hara, Takahito; Yamaoka, Masuo; Kusaka, Masami; Tasaka, Akihiro
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 16 p. 4313 - 4336
反应条件
n-butyllithium in hexane
参考文献
Takeda Chemical Industries, Ltd.
Patent: US6420375 B1, 2002 ;
反应条件
1: 1.) n-BuLi / 1.) Et2O, hexane, 1 h, 2.) 2 h 2: DDQ / tetrahydrofuran / 2 h / Ambient temperature View Scheme
参考文献
Hiyama; Wakasa; Ueda; Kusumoto
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 2 p. 640 - 642
反应条件
potassium permanganate; magnesium sulfate in acetone 2 h;
参考文献
Shishido, Kozo; Yamashita, Akitake; Hiroya, Kou; Fukumoto, Keiichiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 469 - 475
