(E)-3-甲基己-3-烯合成路线 (共 8 条)
反应条件
hydrogen; silica-supported dendrimer-palladium complex (G1-C6-Pd) in methanol
T=25°C; P=724.007 Torr; 3 h; Title compound not separated from byproducts;
参考文献
Zweni, Pumza P.; Alper, Howard
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 6 p. 725 - 731
反应条件
zeolite ZSM-5
T=400°C; P=15201 Torr; 250 h; Fixed bed reactor;
参考文献
Mentzel, Uffe V.; Shunmugavel, Saravanamurugan; Hruby, Sarah L.; Christensen, Claus H.; Holm, Martin S.
Journal of the American Chemical Society, 2009 , vol. 131, # 46 p. 17009 - 17013
反应条件
lithium aluminium tetrahydride
1.) THF, room temperature; Multistep reaction. Title compound not separated from byproducts;
参考文献
Huggins, John M.; Bergman, Robert G.
Journal of the American Chemical Society, 1981 , vol. 103, # 11 p. 3002 - 3011
反应条件
cyclothionine; Na-zeolite; oxygen in hexane
Isomerization;
参考文献
Shailaja; Sivaguru; Robbins, Rebecca J.; Ramamurthy; Sunoj; Chandrasekhar
Tetrahedron, 2000 , vol. 56, # 36 p. 6927 - 6943
反应条件
cyclothionine; Na-zeolite; oxygen in hexane
Isomerization; oxidation; Photolysis; Title compound not separated from byproducts;
参考文献
Shailaja; Sivaguru; Robbins, Rebecca J.; Ramamurthy; Sunoj; Chandrasekhar
Tetrahedron, 2000 , vol. 56, # 36 p. 6927 - 6943
反应条件
lithium
1.) Et2O, r.t.; 2.) Et2O, -40 deg C to r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Maercker; Girreser
Tetrahedron, 1994 , vol. 50, # 27 p. 8019 - 8034
反应条件
lithium; dimethyl sulfate
1.) Et2O, r.t., 664 h; 2.) Et2O, -40 deg C to r.t.; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Maercker; Girreser
Tetrahedron, 1994 , vol. 50, # 27 p. 8019 - 8034
反应条件
cyclothionine; Na-zeolite; oxygen in hexane
Isomerization;
参考文献
Shailaja; Sivaguru; Robbins, Rebecca J.; Ramamurthy; Sunoj; Chandrasekhar
Tetrahedron, 2000 , vol. 56, # 36 p. 6927 - 6943