4'-甲基伞形酮-2-乙酰氨基-3,4,6-三-乙酰基-2-脱氧-beta-D-吡喃葡萄糖苷合成路线 (共 3 条)
反应条件
1: With sodium methylate in methanol; dichloromethane T=20°C; 4 h; 2: in methanol; dichloromethane
参考文献
Carbohydrate Research, , vol. 346, # 12 p. 1467 - 1478
反应条件
1: 7-hydroxy-4-methyl-coumarin With CsOH; tetrabutylammomium bromide in dichloromethane; water
T=20°C; 0.166667 h;
2: 2-Deoxy-2-acetamido-3,4,6-tri-O-acetyl-α-D-glucopyranosyl chloride in dichloromethane; water
0.916667 h;
参考文献
Gold, Henrik; Munneke, Stefan; Dinkelaar, Jasper; Overkleeft, Herman S.; Aerts, Johannes M.F.G.; Codee, Jeroen D.C.; Van Der Marel, Gijs A.
Carbohydrate Research, 2011 , vol. 346, # 12 p. 1467 - 1478
反应条件
triethylamine in dichloromethane
T=20°C; 2 h;
参考文献
Whitworth, Garrett E.; Macauley, Matthew S.; Stubbs, Keith A.; Dennis, Rebecca J.; Taylor, Edward J.; Davies, Gideon J.; Greig, Ian R.; Vocadlo, David J.
Journal of the American Chemical Society, 2007 , vol. 129, # 3 p. 635 - 644