(R)-1-(1-萘基)乙胺合成路线 （共 75 条）
反应条件
1: With (S)-isopropylidene glycerol 3-carboxy-2-naphthoate in methanol T=20°C; 2: With sulfuric acid in ethyl acetate
参考文献
Pallavicini, Marco; Bolchi, Cristiano; Fumagalli, Laura; Valoti, Ermanno; Villa, Luigi
Tetrahedron Asymmetry, 2002 , vol. 13, # 20 p. 2277 - 2282
反应条件
1: With trimethylsilyl iodide in acetonitrile T=20°C; 2: With hydrogenchloride in diethyl ether; water 3: With potassium hydroxide in water
参考文献
Denmark, Scott E.; Nakajima, Noriyuki; Stiff, Cory M.; Nicaise, Olivier J.-C.; Kranz, Michael
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 7-8 p. 1023 - 1045
反应条件
in various solvent(s) T=30°C; 141 h; protease subtilisin Carlsberg;
参考文献
Kitaguchi, Hiroshi; Fitzpatrick, Paul A.; Huber, Joel E.; Klibanov, Alexander M.
Journal of the American Chemical Society, 1989 , vol. 111, # 8 p. 3094 - 3095
反应条件
lead(IV) acetate in methanol; dichloromethane T=0°C; 0.0666667 h;
参考文献
Pridgen, Lendon N.; Mokhallalati, Mohamed K.; Wu, Ming-Jung
Journal of Organic Chemistry, 1992 , vol. 57, # 4 p. 1237 - 1241
反应条件
heptakis-(6-O-TIPS)-β-CD; triethylamine in cyclohexane T=10°C; 6 h; Resolution of racemate; enantioselective reaction;
参考文献
Asahara, Haruyasu; Kida, Toshiyuki; Iwamoto, Takuya; Hinoue, Tomoaki; Akashi, Mitsuru
Tetrahedron, 2014 , vol. 70, # 2 p. 197 - 203
反应条件
heptakis-(6-O-TIPS)-β-CD; triethylamine in cyclohexane T=10°C; 6 h; Resolution of racemate; enantioselective reaction;
参考文献
Asahara, Haruyasu; Kida, Toshiyuki; Iwamoto, Takuya; Hinoue, Tomoaki; Akashi, Mitsuru
Tetrahedron, 2014 , vol. 70, # 2 p. 197 - 203
反应条件
heptakis-(6-O-TIPS)-β-CD; triethylamine in cyclohexane T=10°C; 6 h; Resolution of racemate; enantioselective reaction;
参考文献
Asahara, Haruyasu; Kida, Toshiyuki; Iwamoto, Takuya; Hinoue, Tomoaki; Akashi, Mitsuru
Tetrahedron, 2014 , vol. 70, # 2 p. 197 - 203
反应条件
heptakis-(6-O-TIPS)-β-CD; triethylamine in cyclohexane T=10°C; 6 h; Resolution of racemate; enantioselective reaction;
参考文献
Asahara, Haruyasu; Kida, Toshiyuki; Iwamoto, Takuya; Hinoue, Tomoaki; Akashi, Mitsuru
Tetrahedron, 2014 , vol. 70, # 2 p. 197 - 203
反应条件
heptakis-(6-O-TIPS)-β-CD; triethylamine in cyclohexane T=10°C; 6 h; Resolution of racemate; enantioselective reaction;
参考文献
Asahara, Haruyasu; Kida, Toshiyuki; Iwamoto, Takuya; Hinoue, Tomoaki; Akashi, Mitsuru
Tetrahedron, 2014 , vol. 70, # 2 p. 197 - 203
反应条件
heptakis-(6-O-TIPS)-β-CD; triethylamine in cyclohexane T=10°C; 6 h; Resolution of racemate; enantioselective reaction;
参考文献
Asahara, Haruyasu; Kida, Toshiyuki; Iwamoto, Takuya; Hinoue, Tomoaki; Akashi, Mitsuru
Tetrahedron, 2014 , vol. 70, # 2 p. 197 - 203
