二乙基6,6'-二氰基-2,2'-联吡啶-4,4'-二羧酸酯合成路线 （共 2 条）
反应条件
1: 4,4'-bis(ethoxycarbonyl)-2,2'-bipyridine-N,N'-dioxide With dimethyl sulfate
T=100°C; 4 h;
2: potassium cyanide in water
T=-10°C; 4 h;
参考文献
Renouard, Thierry; Graetzel, Michael
Tetrahedron, 2001 , vol. 57, # 38 p. 8145 - 8150
反应条件
1.1: 95 percent / peracetic acid / acetic acid / 72 h / 40 °C
2.1: Me2SO4 / 4 h / 100 °C
2.2: 55 percent / H2O / 4 h / -10 °C
View Scheme
参考文献
Renouard, Thierry; Graetzel, Michael
Tetrahedron, 2001 , vol. 57, # 38 p. 8145 - 8150
