(9ci)-2-(2-噻吩)-1H-苯并咪唑合成路线 （共 41 条）
反应条件
Na2S2O5 in N,N-dimethyl-formamide
T=80°C; 0.4 h; Microwave irradiation;
参考文献
Secci, Daniela; Bolasco, Adriana; D'Ascenzio, Melissa; Della Sala, Flavio; Yanez, Matilde; Carradori, Simone
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 5 p. 1187 - 1195
反应条件
in N,N-dimethyl-formamide
T=110°C;
参考文献
Shaukat, Awais; Mirza, Hira M.; Ansari, Amna H.; Yasinzai, Masoom; Zaidi, Sohail Z.; Dilshad, Sana; Ansari, Farzana L.
Medicinal Chemistry Research, 2013 , vol. 22, # 8 p. 3606 - 3620
反应条件
2,6-dimethylpyridine; bis(triphenylphosphine)palladium(II)-chloride in N,N-dimethyl acetamide
T=140°C; P=4912.9 Torr; 24 h;
参考文献
Perry; Wilson
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7016 - 7021
参考文献
Schiffmann, Rolf; Neugebauer, Alexander; Klein, Christian D.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 2 p. 511 - 522
反应条件
copper(ll) bromide in toluene
T=100°C; 24 h;
参考文献
Xiao, Tiebo; Xiong, Shengwei; Xie, Yang; Dong, Xichang; Zhou, Lei
RSC Advances, 2013 , vol. 3, # 36 p. 15592 - 15595
反应条件
1: With Pd(2,2,6,6-tetrametyl-3,5-heptanedionate)2; toluene-4-sulfonic acid in ethyl acetate
T=80°C; 1 h;
2: With hydrogen in ethyl acetate
T=80°C; P=25858.1 Torr; 7 h;
参考文献
Bhor, Malhari D.; Bhanage, Bhalchandra M.
Synthetic Communications, 2010 , vol. 40, # 12 p. 1743 - 1749
反应条件
air; silica gel
0.116667 h; Microwave irradiationneat (no solvent);
参考文献
Yu, Chuanming; Guo, Peng; Jin, Can; Su, Weike
Journal of Chemical Research, 2009 , # 5 p. 333 - 336
反应条件
potassium tert-butylate in N,N-dimethyl acetamide
T=100°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Xiang, Shi-Kai; Tan, Wen; Zhang, Dong-Xue; Tian, Xian-Li; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 42 p. 7271 - 7275
反应条件
sodium azide; N,N,N',N,-tetramethylethylenediamine; copper(l) chloride in dimethyl sulfoxide
T=120°C; 12 h;
参考文献
Kim, Yong; Kumar, Manian Rajesh; Park, Namjin; Heo, Yumi; Lee, Sunwoo
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9577 - 9583
反应条件
potassium carbonate in water
T=100°C; 30 h; Schlenk techniqueGreen chemistry;
参考文献
Chen, Chunxia; Chen, Chen; Li, Bin; Tao, Jingwei; Peng, Jinsong
Molecules, 2012 , vol. 17, # 11 p. 12506 - 12520
