2-甲基-1,2,3,4-四氢萘合成路线 （共 32 条）
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
16 h; Heating;
参考文献
Beckwith, Athelstan L. J.; Gerba, Sendaba
Australian Journal of Chemistry, 1992 , vol. 45, # 1 p. 289 - 308
反应条件
1: nPrCO2Na
2: P, aq. HI / 48 h / Heating
3: SOCl2
4: H2 / Pd
5: (i) N2H4, Et2O, (ii) HgO, Na2SO4, KOH, Et2O, EtOH
6: hexane / -60 °C / Irradiation
View Scheme
参考文献
Gutsche,C.D. et al.
Tetrahedron, 1962 , vol. 18, p. 617 - 627
反应条件
hydrogen; copper(l) chloride; zinc(II) chloride
T=400°C;
参考文献
Nakatsuyi,Y. et al.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 618 - 624
反应条件
1: 78 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature
2: 0.25 h / Ambient temperature
3: LiBr, hexamethylphosphoric triamide (HMPA) / tetrahydrofuran / 6 h / Heating
4: 57 percent / tributylstannane, azobisisobutyronitrile / benzene / 16 h / Heating
View Scheme
参考文献
Beckwith, Athelstan L. J.; Gerba, Sendaba
Australian Journal of Chemistry, 1992 , vol. 45, # 1 p. 289 - 308
反应条件
1: 0.25 h / Ambient temperature
2: LiBr, hexamethylphosphoric triamide (HMPA) / tetrahydrofuran / 6 h / Heating
3: 57 percent / tributylstannane, azobisisobutyronitrile / benzene / 16 h / Heating
View Scheme
参考文献
Beckwith, Athelstan L. J.; Gerba, Sendaba
Australian Journal of Chemistry, 1992 , vol. 45, # 1 p. 289 - 308
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Madinaveitia
Anales de la Real Sociedad Espanola de Fisica y Quimica, 1934 , vol. 32, p. 1100,1105
Chem. Zentralbl., 1935 , vol. 106, # I p. 3134
参考文献
Franz, James A.; Camaioni, Donald M.
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5247 - 5255
反应条件
T=327°C; P=0.01 Torr; flash vacuum pyrolysis, other reaction temperatures; Product distribution;
参考文献
Franz, James A.; Camaioni, Donald M.
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5247 - 5255
反应条件
T=427°C; P=0.01 Torr; flash vacuum pyrolysis, other reaction temperatures; Product distribution;
参考文献
Franz, James A.; Camaioni, Donald M.
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5247 - 5255
反应条件
T=427°C; P=0.01 Torr; flash vacuum pyrolysis, other reaction temperatures; Product distribution;
参考文献
Franz, James A.; Camaioni, Donald M.
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5247 - 5255
