2-乙酰基环戊烷-1,3-二酮合成路线 （共 10 条）
反应条件
acetic acid T=100°C; 24 h;
参考文献
Nilsson, Martin
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1981 , vol. 35, # 9 p. 667 - 668
反应条件
hydrogenchloride in ethanol
参考文献
Zaidan Hojin Biseibutsu Kagaku Kenkyu Kai
Patent: US4003936 A1, 1977 ;
反应条件
triethylsilane; boron trifluoride diethyl etherate in trifluoroacetic acid Ambient temperature;
参考文献
Akhrem, A. A.; Lakhvich, F. A.; Lis, L. G.; Khripach, V. A.; Fil'chenkov, N. A.; Kozinets, V. A.
Doklady Chemistry, 1990 , vol. 311, # 4 p. 79 - 80
Dokl. Akad. Nauk SSSR Ser. Khim., 1990 , vol. 311, # 6 p. 1381 - 1384
反应条件
Barium in tetrahydrofuran
6 h; Heating;
参考文献
Lim, Sunkwon; Min, Yosep; Choi, Bohyun; Kim, Daesig; Yoon, Il; Lee, Shim Sung; Lee, Ik-Mo
Tetrahedron Letters, 2001 , vol. 42, # 43 p. 7645 - 7649
反应条件
aluminium trichloride in 1,2-dichloro-ethane
T=15°C; 3 h; other 2-acyloxy-2-cyclopenten-1-ones; Product distribution;
参考文献
Lakhvich, F. A.; Khlebnikova, T. S.; Akhrem, A. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 12.1 p. 2280 - 2286
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 12 p. 2541 - 2549
反应条件
potassium tert-butylate in benzene
参考文献
Vandewalle,M.
Bulletin des Societes Chimiques Belges, 1964 , vol. 73, p. 628 - 633
反应条件
1: pyridine / chloroform
2: 2-hydroxy-2-methyl-propionitrile; triethylamine / acetonitrile / 16 h / 20 °C
View Scheme
参考文献
Khlebnikova; Piven'; Lakhvich
Russian Journal of General Chemistry, 2014 , vol. 84, # 3 p. 465 - 473
反应条件
aluminium trichloride in 1,2-dichloro-ethane
参考文献
Merenyi,F.; Nilsson,M.
Acta Chemica Scandinavica (1947-1973), 1967 , vol. 21, p. 1755 - 1758
参考文献
Shestak; Novikov; Prokof'eva; Chaikina
Pharmaceutical Chemistry Journal, 1999 , vol. 33, # 12 p. 631 - 634
反应条件
aluminium trichloride
参考文献
Merenyi,F.; Nilsson,M.
Acta Chemica Scandinavica (1947-1973), 1964 , vol. 18, p. 1368 - 1372
