3-羟基-1-金刚烷甲醇合成路线 （共 13 条）
参考文献
Daichel Chemical Industries Ltd
Patent: EP1000924 A1, 2000 ;
参考文献
Daicel Chemical Industries, Ltd.; Ishii, Yasutaka
Patent: EP915077 A1, 1999 ;
参考文献
Daicel Chemical Industries, Ltd.; Ishii, Yasutaka
Patent: EP915077 A1, 1999 ;
反应条件
2,2'-azo-bisisobutyronitrile; n-Bu4NBH3CN in acetonitrile T=80°C; 6 h; Inert atmosphere;
参考文献
Kawamoto, Takuji; Fukuyama, Takahide; Ryu, Ilhyong
Journal of the American Chemical Society, 2012 , vol. 134, # 2 p. 875 - 877
反应条件
nickel; hydrazine hydrate in isopropyl alcohol 10 h; Heating;
参考文献
Klimochkin, Yu. N.; Zhilkina, E. O.; Abramov, O. V.; Moiseev, I. K.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 7.1 p. 1126 - 1131
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 7 p. 1358 - 1364
反应条件
triethylamine in 1,4-dioxane
参考文献
Stepanov,F.N. et al.
Zhurnal Organicheskoi Khimii, 1971 , vol. 8, # 6 p. 1179 - 1183,1192 - 1196
反应条件
1: CHCl3 2: KOH / methanol View Scheme
参考文献
Stepanov,F.N. et al.
Zhurnal Organicheskoi Khimii, 1971 , vol. 8, # 6 p. 1179 - 1183,1192 - 1196
反应条件
1: 65 percent / 100percent HNO3 / 3 h / 20 °C 2: 84 percent / 60percent aq. AcOH, 60percent aq. HNO3 / 5 h / 85 °C 3: 80 percent / NH2NH2*H2O, Raney-Ni / propan-2-ol / 10 h / Heating View Scheme
参考文献
Klimochkin, Yu. N.; Zhilkina, E. O.; Abramov, O. V.; Moiseev, I. K.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 7.1 p. 1126 - 1131
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 7 p. 1358 - 1364
反应条件
1: 1.) 100percent HNO3, AcOH, 2.) 30percent aq. AcOH / 1.) 20 deg C, 0.5 h, 2.) reflux, 0.5 h 2: 85 percent / 100percent HNO3, Ac2O / 5 h / 20 °C 3: 75 percent / 60percent aq. AcOH, 60percent aq. HNO3 / 5 h / 85 °C 4: 80 percent / NH2NH2*H2O, Raney-Ni / propan-2-ol / 10 h / Heating View Scheme
参考文献
Klimochkin, Yu. N.; Zhilkina, E. O.; Abramov, O. V.; Moiseev, I. K.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 7.1 p. 1126 - 1131
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 7 p. 1358 - 1364
反应条件
1: 85 percent / 100percent HNO3, Ac2O / 5 h / 20 °C 2: 75 percent / 60percent aq. AcOH, 60percent aq. HNO3 / 5 h / 85 °C 3: 80 percent / NH2NH2*H2O, Raney-Ni / propan-2-ol / 10 h / Heating View Scheme
参考文献
Klimochkin, Yu. N.; Zhilkina, E. O.; Abramov, O. V.; Moiseev, I. K.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 7.1 p. 1126 - 1131
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 7 p. 1358 - 1364
