5-甲基-2-硝基苯甲醚合成路线 （共 55 条）
反应条件
sodium hydroxide; sulfur
参考文献
Khotinsky; Jacopson-Jacopmann
Chemische Berichte, 1909 , vol. 42, p. 3101
反应条件
1: 73 percent / potassium permanganate, sodium hydrogen carbonate / H2O / 4 h / Heating 2: 91 percent / BF3 / 12 h View Scheme
参考文献
Baret, Paul; Beaujolais, Virginie; Beguin, Claude; Gaude, Didier; Pierre, Jean-Louis; Serratrice, Guy
European Journal of Inorganic Chemistry, 1998 , # 5 p. 613 - 619
反应条件
potassium permanganate; sodium carbonate in water 1.5 h; Heating;
参考文献
Ismail, Ibrahim A.; Sharp, Dale E.; Chedekel, Miles R.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2243 - 2246
反应条件
1: 73 percent / potassium permanganate, sodium hydrogen carbonate / H2O / 4 h / Heating 2: 91 percent / BF3 / 12 h 3: 91 percent / hydrogen / 10percent Pd/C / CH2Cl2; ethanol / 12 h View Scheme
参考文献
Baret, Paul; Beaujolais, Virginie; Beguin, Claude; Gaude, Didier; Pierre, Jean-Louis; Serratrice, Guy
European Journal of Inorganic Chemistry, 1998 , # 5 p. 613 - 619
反应条件
1: KMnO4 / H2O / Heating 2: SOCl2 3: (i) Mg, (ii) H2SO4, AcOH 4: Br2 / acetic acid View Scheme
参考文献
Julia,M.; Chastrette,F.
Bulletin de la Societe Chimique de France, 1962 , p. 2255 - 2261
反应条件
1: aqueous formaldehyde; concentrated aqueous HCl / Einleiten von HCl 2: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Matsukawa; Matsuno; Shirakawa
Yakugaku Zasshi, 1943 , vol. 63, p. 1,4
Chem.Abstr., 1950 , p. 7255
反应条件
1.1: SnCl2·2H2O / methanol / 3 h / Reflux 1.2: pH 8 2.1: copper(ll) bromide; tert.-butylnitrite / acetonitrile / 0.33 h / 65 °C / Inert atmosphere 3.1: tert.-butyl lithium / pentane; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere 3.2: 2 h / -78 - 20 °C View Scheme
参考文献
KATHOLIEKE UNIVERSITEIT LEUVEN
Patent: US2012/316161 A1, 2012 ;
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 72 h; Heating;
参考文献
Ismail, Ibrahim A.; Sharp, Dale E.; Chedekel, Miles R.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2243 - 2246
反应条件
1: 73 percent / potassium permanganate, sodium hydrogen carbonate / H2O / 4 h / Heating 2: 91 percent / BF3 / 12 h 3: 91 percent / hydrogen / 10percent Pd/C / CH2Cl2; ethanol / 12 h 4: 20percent H2SO4, sodium nitrite / H2O / 0 °C 5: KI / H2O / 2 h / 50 °C View Scheme
参考文献
Baret, Paul; Beaujolais, Virginie; Beguin, Claude; Gaude, Didier; Pierre, Jean-Louis; Serratrice, Guy
European Journal of Inorganic Chemistry, 1998 , # 5 p. 613 - 619
反应条件
sodium hydroxide; tert-butyl alcohol in water Irradiation; Quantum yield;
参考文献
Sawaura, Masaki; Mukai, Toshio
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3213 - 3214
