3-乙氧基羰基-1-叔丁基戊烷-1,4-二酮合成路线 （共 9 条）
反应条件
1: aqueous potassium carbonate-solution 2: aqueous KOH-solution View Scheme
参考文献
Messina; Brown
Journal of the American Chemical Society, 1952 , vol. 74, p. 1087
反应条件
potassium carbonate in acetone
48 h; Heating;
参考文献
Chiu, Pak-Han; Sammes, Michael P.
Tetrahedron, 1990 , vol. 46, # 10 p. 3439 - 3456
参考文献
Messina; Brown
Journal of the American Chemical Society, 1952 , vol. 74, p. 920,922
反应条件
sodium iodide in acetone
10 h; Heating; Yield given;
参考文献
Trahanovsky, Walter S.; Chou, Chin-Hsing; Cassady, Timothy J.
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2613 - 2615
反应条件
1: copper(II) sulfate / cyclohexane / 14 h / Heating
2: 2 M HCl / diethyl ether / 12 h / Ambient temperature
View Scheme
参考文献
Saigo, Kazuhiko; Kurihara, Hiroshi; Miura, Hisao; Hongu, Akinori; Kubota, Naomi; et al.
Synthetic Communications, 1984 , vol. 14, # 9 p. 787 - 796
反应条件
1: 74 percent / 1.) NaH / benzene / 1.) 10 deg C, 1 h, room temperature, 2 h, 2.) 6 h
2: copper(II) sulfate / cyclohexane / 14 h / Heating
3: 2 M HCl / diethyl ether / 12 h / Ambient temperature
View Scheme
参考文献
Saigo, Kazuhiko; Kurihara, Hiroshi; Miura, Hisao; Hongu, Akinori; Kubota, Naomi; et al.
Synthetic Communications, 1984 , vol. 14, # 9 p. 787 - 796
反应条件
sodium hydride
1.) dimethoxyethane, 2.) dimethoxyethane, reflux, 15 h; Multistep reaction;
参考文献
Smith, Jonathan O.; Mandal, Braja K.
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 5 p. 1441 - 1446
参考文献
Trahanovsky, Walter S.; Chou, Chin-Hsing; Cassady, Timothy J.
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2613 - 2615
参考文献
Smith, Jonathan O.; Mandal, Braja K.
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 5 p. 1441 - 1446
