1,2-二氯-4-(甲基磺酰基)苯合成路线 (共 8 条)
反应条件
potassium hydroxide T=190 - 195°C;
参考文献
Gen. Aniline and Film Corp.
Patent: US2314379 , 1940 ;
Full Text Show Details
I.G. Farbenind.
Patent: DE739571 , 1939 ;
DRP/DRBP Org.Chem.
反应条件
ammonia; water T=200°C;
参考文献
I.G.Farbenind.
Patent: FR829926 , 1937 ;
反应条件
dihydrogen peroxide in water
T=75°C; 1.75 h;
参考文献
Jereb, Marjan
Green Chemistry, 2012 , vol. 14, # 11 p. 3047 - 3052,6
Title/Abstract Full Text Show Details
Jereb, Marjan
Green Chemistry, 2012 , vol. 14, # 11 p. 3047 - 3052
反应条件
trifluorormethanesulfonic acid; bismuth(III) chloride
T=130°C; Friedel-Crafts reaction; 168 h;
参考文献
Peyronneau, Magali; Boisdon, Marie-Therese; Roques, Nicolas; Mazieres, Stephane; Le Roux, Christophe
European Journal of Organic Chemistry, 2004 , # 22 p. 4636 - 4640
反应条件
trifluorormethanesulfonic acid; Boron tris(trifluoromethanesulfonate)
T=20°C; Substitution; 4 h;
参考文献
Olah; Orlinkov; Oxyzoglou; Prakash, G.K. Suria
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 11 p. 1573 - 1578
反应条件
SbF5
T=0°C; Substitution; 0.5 h; Further byproducts given;
参考文献
Olah; Orlinkov; Oxyzoglou; Prakash, G.K. Suria
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 11 p. 1573 - 1578
反应条件
1: ethanol
2: aqueous hydrogen peroxide; acetic acid
View Scheme
参考文献
Dandin et al.
Journal of the Karnatak University, 1956 , vol. 1, p. 64,68
反应条件
chlorosulphuric acid; iodine; chlorine
参考文献
Farbw. Hoechst
Patent: DE949054 , 1954 ;