ALPHA-氯-4-甲氧基苯甲醛肟合成路线 （共 51 条）
反应条件
hydrogenchloride; Oxonereg;; silica gel T=20°C; 0.15 h;
参考文献
Bigdeli, Mohammad A.; Mahdavinia, Gholam Hossein; Jafari, Saeed
Journal of Chemical Research, 2007 , # 1 p. 26 - 28
反应条件
hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; chlorine 1.) 30 min, 2.) 0 deg C; Yield given. Multistep reaction;
参考文献
Wielkopolski; Smieszek; Witek; Dabrowski; Wieczorek; Lejczak; Kafarski
Pesticide Science, 1994 , vol. 40, # 2 p. 107 - 112
反应条件
diethyl ether; nitrosyl chloride
参考文献
Kinney et al.
Journal of the American Chemical Society, 1933 , vol. 55, p. 3418,3421
反应条件
thionyl chloride; ethanol 1.) CCl4; 2.) room temp; Yield given. Multistep reaction;
参考文献
Uchida, Yuzuru; Kozuka, Seizi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 4 p. 2011 - 2012
参考文献
Kinney et al.
Journal of the American Chemical Society, 1933 , vol. 55, p. 3418,3421
反应条件
in geschlossenem Gefaess unter starker Kuehlung;
参考文献
Kinney et al.
Journal of the American Chemical Society, 1933 , vol. 55, p. 3418,3421
反应条件
diethyl ether; ammonia
参考文献
Kinney et al.
Journal of the American Chemical Society, 1933 , vol. 55, p. 3418,3421
反应条件
triethylamine in diethyl ether T=20°C; 12 h;
参考文献
Baird, Mark S; Huber, Florian A.M; Clegg, William
Tetrahedron, 2001 , vol. 57, # 49 p. 9849 - 9858
反应条件
1: triethylamine / dichloromethane / 2 h / 20 °C 2: carbon tetrabromide; triphenylphosphine / dichloromethane / 1 h / Cooling with ice View Scheme
参考文献
Daiichi Sankyo Company, Limited
Patent: EP2308838 A1, 2011 ;
反应条件
in ethyl acetate; toluene
参考文献
Hansen, Eric C.; Levent, Mahmut; Connolly, Terrence J.
Organic Process Research and Development, 2010 , vol. 14, # 3 p. 574 - 578
