N-(4-溴苯基)-3-氧丁酰胺合成路线 (共 18 条)
反应条件
Acylation; 0.316667 h; microwave irradiation;
参考文献
Suri; Satti
Synthetic Communications, 2000 , vol. 30, # 20 p. 3709 - 3718
反应条件
in toluene T=90°C; 5 h;
参考文献
Boehringer Ingelheim International GmbH
Patent: US2005/267115 A1, 2005 ;
Location in patent: Page/Page column 21 ;
US 20050267115 A1
反应条件
in toluene; Petroleum ether
参考文献
Burroughs Wellcome Co.
Patent: US4587341 A1, 1986 ;
反应条件
in acetonitrile T=160°C; 0.5 h; Microwave irradiation;
参考文献
Wlodarczyk, Nicolas; Simenel, Catherine; Delepierre, Muriel; Barale, Jean-Christophe; Janin, Yves L.
Synthesis, 2011 , # 6 art. no. T51110SS, p. 934 - 942
反应条件
acetic acid in acetonitrile T=130°C; 0.5 h; Microwave irradiation;
参考文献
Wlodarczyk, Nicolas; Simenel, Catherine; Delepierre, Muriel; Barale, Jean-Christophe; Janin, Yves L.
Synthesis, 2011 , # 6 art. no. T51110SS, p. 934 - 942
反应条件
toluene-4-sulfonic acid in acetonitrile T=130°C; 0.5 h; Microwave irradiation;
参考文献
Wlodarczyk, Nicolas; Simenel, Catherine; Delepierre, Muriel; Barale, Jean-Christophe; Janin, Yves L.
Synthesis, 2011 , # 6 art. no. T51110SS, p. 934 - 942
反应条件
in acetonitrile T=200°C; 1 h; Microwave irradiation;
参考文献
Wlodarczyk, Nicolas; Simenel, Catherine; Delepierre, Muriel; Barale, Jean-Christophe; Janin, Yves L.
Synthesis, 2011 , # 6 art. no. T51110SS, p. 934 - 942
反应条件
in acetonitrile T=130°C; 1 h; Microwave irradiation;
参考文献
Wlodarczyk, Nicolas; Simenel, Catherine; Delepierre, Muriel; Barale, Jean-Christophe; Janin, Yves L.
Synthesis, 2011 , # 6 art. no. T51110SS, p. 934 - 942
反应条件
in acetonitrile T=130°C; 0.5 h; Microwave irradiationMolecular sieve;
参考文献
Wlodarczyk, Nicolas; Simenel, Catherine; Delepierre, Muriel; Barale, Jean-Christophe; Janin, Yves L.
Synthesis, 2011 , # 6 art. no. T51110SS, p. 934 - 942
反应条件
in acetonitrile T=130°C; 0.5 h; Microwave irradiation;
参考文献
Wlodarczyk, Nicolas; Simenel, Catherine; Delepierre, Muriel; Barale, Jean-Christophe; Janin, Yves L.
Synthesis, 2011 , # 6 art. no. T51110SS, p. 934 - 942