3,4,5-三甲氧基苄氯合成路线 （共 34 条）
反应条件
thionyl chloride in dichloromethane T=0 - 23°C;
参考文献
Percec, Virgil; Won, Betty C.; Peterca, Mihai; Heiney, Paul A.
Journal of the American Chemical Society, 2007 , vol. 129, # 36 p. 11265 - 11278
反应条件
1: LiAlH4; diethyl ether 2: aqueous HCl View Scheme
参考文献
Schwachhofer,G.; Chopin,J.
Bulletin de la Societe Chimique de France, 1962 , p. 835 - 843
反应条件
1: NaBH4 / methanol / 20 °C 2: SOCl2 / dioxane / 20 °C View Scheme
参考文献
Cook et al.
Journal of the Chemical Society, 1944 , p. 322,324
反应条件
chloromethyl methyl sulfide; tin(IV) chloride Yield given;
参考文献
Ohira, Susumi; Shirane, Fukue; Nozaki, Hiroshi; Yahiro, Shigeru; Nakayama, Mitsuru
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 7 p. 2427 - 2428
反应条件
1: sodium ethylate; ethanol 2: N.N-dimethyl-aniline; SOCl2 / 0 °C / zuletzt bei 100grad View Scheme
参考文献
Cook et al.
Journal of the Chemical Society, 1944 , p. 322,324
反应条件
1: tetrachloroethane; SnCl2; etheric HCl / 0 °C / Erhitzen des Reaktionsprodukts mit wss.HCl und Essigsaeure 2: ethanol; platinum / Hydrogenation 3: N.N-dimethyl-aniline; SOCl2 / 0 °C / zuletzt bei 100grad View Scheme
参考文献
Cook et al.
Journal of the Chemical Society, 1944 , p. 322,324
反应条件
in toluene 24 h; RefluxInert atmosphere;
参考文献
Dakdouki, Saada C.; Villemin, Didier; Bar, Nathalie
European Journal of Organic Chemistry, 2010 , # 2 p. 333 - 337
反应条件
1: dimethyl sulfoxide 2: potassium hydroxide; water / ethanol / 15 h / |Reflux 3: lithium aluminium tetrahydride / tetrahydrofuran / 3.5 h / 20 °C / |Reflux View Scheme
参考文献
Zheng, Cheng; Guo, Yibing; Meng, Ying; Dou, Sufeng; Shao, Jian; Yang, Yumin
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 5 p. 654 - 664
反应条件
in tetrahydrofuran 4 h; Reflux;
参考文献
Zhang, Cunlong; Tan, Chunyan; Zu, Xuyu; Zhai, Xin; Liu, Feng; Chu, Bizhu; Ma, Xiaohua; Chen, Yuzong; Gong, Ping; Jiang, Yuyang
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 4 p. 1404 - 1414
参考文献
Nippon Chemiphar Co., Ltd.
Patent: US5070089 A1, 1991 ;
