反应条件
chloro-trimethyl-silane; iodine; magnesium; sodium iodide
1.) THF, 20 deg C, 4 h then 22 deg C, 3 h; 2.) CH3CN, 10 deg C, 3.5 h then up to r.t., 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Stoner, Eric J.; Cothron, Darlene A.; Balmer, Mary K.; Roden, Brian A.
Tetrahedron, 1995 , vol. 51, # 41 p. 11043 - 11062