1-甲基-4-(三氟甲基磺酰基)苯合成路线 （共 10 条）
反应条件
sulfuric acid; nitric acid
参考文献
Yagupol'skii,L.M. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1965 , vol. 35, # 2 p. 377 - 387,377 - 385
反应条件
N-bromosuccinmide in tetrachloromethane 10 h; HeatingIrradiation;
参考文献
Goumont, Regis; Faucher, Nicolas; Moutiers, Gilles; Tordeux, Marc; Wakselman, Claude
Synthesis, 1997 , # 6 p. 691 - 695
反应条件
1,10-phenanthroline; tetrabutyl ammonium fluoride; cupric trifluoroacetate in dimethyl sulfoxide
T=130°C; 8 h; Inert atmosphereSealed tube;
参考文献
Lin, Xiaoxi; Wang, Guimei; Li, Huaifeng; Huang, Yuanyuan; He, Weiming; Ye, Dandan; Huang, Kuo-Wei; Yuan, Yaofeng; Weng, Zhiqiang
Tetrahedron, 2013 , vol. 69, # 12 p. 2628 - 2632
反应条件
dihydrogen peroxide in acetic acid
T=50°C; 48 h;
参考文献
Goumont, Regis; Faucher, Nicolas; Moutiers, Gilles; Tordeux, Marc; Wakselman, Claude
Synthesis, 1997 , # 6 p. 691 - 695
反应条件
tris(dimethylamino)-sulphonium difluorotrimethylsilicate in Petroleum ether
T=25°C; 0.5 h;
参考文献
Kolomeitsev; Movchun; Kondratenko; Yagupolski
Synthesis, 1990 , # 12 p. 1151 - 1152
反应条件
in diethyl ether
T=-78°C;
参考文献
Creary, Xavier
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2727 - 2729
反应条件
aluminium trichloride in benzene
25°C;
参考文献
Hendrickson, J. B.; Bair, K. W.
J. Org. chem., 1977 , vol. 42, p. 3875 - 3878
反应条件
1: HF / 100 - 160 °C
2: CrO3; glacial acetic acid / 100 - 130 °C
View Scheme
参考文献
Gen. Aniline Works
Patent: US2108606 , 1937 ;
Full Text Show Details
I.G. Farbenind.
Patent: DE682971 , 1936 ;
DRP/DRBP Org.Chem.
参考文献
Sekiya, Akira; Umemoto, Teruo
Chemistry Letters, 1982 , p. 1519 - 1520
反应条件
ammonia
Irradiation;
参考文献
Kondratenko,N.V. et al.
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, # 10 p. 2235,2086 - 2087
