6-甲基庚-6-烯-2-基乙酸酯合成路线 （共 13 条）
反应条件
trifluoroacetic acid in nitromethane T=0°C; 1.5 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
1: TFA / nitromethane / 1.5 h / 0 °C 2: POCl3 / pyridine / 15 h / Ambient temperature View Scheme
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
1: 82 percent / HBF4 / CH2Cl2; diethyl ether / 0.5 h / -30 °C 2: t-BuOK / dimethylsulfoxide / 24 h / 20 °C View Scheme
参考文献
Badet, B.; Julia, M.; Mallet, J. M.; Schmitz, C.
Tetrahedron Letters, 1983 , vol. 24, # 30 p. 4331 - 4334
反应条件
trifluoroacetic acid in nitromethane T=0°C; 1.5 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
1: TFA / nitromethane / 1.5 h / 0 °C 2: POCl3 / pyridine / 15 h / Ambient temperature View Scheme
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
sodium hydroxide in methanol
参考文献
Badet, B.; Julia, M.; Mallet, J. M.; Schmitz, C.
Tetrahedron Letters, 1983 , vol. 24, # 30 p. 4331 - 4334
反应条件
1: HBF4*Et2O / CH2Cl2 / -30 °C 2: methanol 3: t-BuOK / dimethylsulfoxide / 24 h / Ambient temperature View Scheme
参考文献
Badet, B.; Julia, M.; Mallet, J. M.; Schmitz, C.
Tetrahedron Letters, 1983 , vol. 24, # 30 p. 4331 - 4334
反应条件
1: HBF4*Et2O / CH2Cl2 / -30 °C 2: methanol 3: t-BuOK / dimethylsulfoxide / 24 h / Ambient temperature View Scheme
参考文献
Badet, B.; Julia, M.; Mallet, J. M.; Schmitz, C.
Tetrahedron Letters, 1983 , vol. 24, # 30 p. 4331 - 4334
反应条件
trichlorophosphate in pyridine
15 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
1: H2SO4
2: NaH
View Scheme
参考文献
Muntyan,G.E. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1972 , vol. 21, p. 861 - 865
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1972 , vol. 21, # 4 p. 909 - 914
