环氧十五烷-2,13-二酮合成路线 （共 15 条）
反应条件
ozone in methanol; dichloromethane
1 h; Yield given;
参考文献
Milenkov, Branimir; Guggisberg, Armin; Hesse, Manfred
Helvetica Chimica Acta, 1987 , vol. 70, p. 760 - 765
反应条件
1: 97 percent / KHCO3 / methanol / 96 h
2: 64 percent / NaH, 4 Angstroem molecular sieves / dimethylformamide / 1.5 h / 20 °C
3: O3 / CH2Cl2; methanol / 1 h
View Scheme
参考文献
Milenkov, Branimir; Guggisberg, Armin; Hesse, Manfred
Helvetica Chimica Acta, 1987 , vol. 70, p. 760 - 765
反应条件
1: 64 percent / NaH, 4 Angstroem molecular sieves / dimethylformamide / 1.5 h / 20 °C
2: O3 / CH2Cl2; methanol / 1 h
View Scheme
参考文献
Milenkov, Branimir; Guggisberg, Armin; Hesse, Manfred
Helvetica Chimica Acta, 1987 , vol. 70, p. 760 - 765
反应条件
dimethylsulfide; trifluoromethylsulfonic anhydride; ozone; N-ethyl-N,N-diisopropylamine
Yield given. Multistep reaction;
参考文献
Hanaki, Naoyuki; Ishihara, Kazuaki; Kaino, Makoto; Naruse, Yuji; Yamamoto, Hisashi
Tetrahedron, 1996 , vol. 52, # 21 p. 7297 - 7320
反应条件
hydroxylamine hydrochloride; sodium carbonate in methanol; water
4 h; Reflux;
参考文献
Meng, Xiang-Qing; Zhang, Jian-Jun; Liang, Xiao-Mei; Zhu, Wei-Juan; Dong, Yan-Hong; Wu, Xue-Min; Huang, Jia-Xing; Rui, Chang-Hui; Fan, Xian-Lin; Chen, Fu-Heng; Wang, Dao-Quan
Journal of Agricultural and Food Chemistry, 2009 , vol. 57, # 2 p. 610 - 617
