苯基2,3,4,6-四-O-苄基-1-硫代-beta-D-吡喃葡萄糖苷合成路线 （共 16 条）
反应条件
tetra-n-butylammonium tetrafluoroborate; potassium carbonate in acetonitrile Ambient temperatureelectrolyse; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Aloui; Fairbanks
Synlett, 2001 , # 6 p. 797 - 799
反应条件
tetra-n-butylammonium tetrafluoroborate; potassium carbonate in acetonitrile Ambient temperatureelectrolyse; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Aloui; Fairbanks
Synlett, 2001 , # 6 p. 797 - 799
反应条件
naphthalenyllithium in tetrahydrofuran T=-78°C; 0.25 h; Yield given;
参考文献
Lancelin, Jean-Marc; Morin-Allory, Luc; Sinay, Pierre
Journal of the Chemical Society, Chemical Communications, 1984 , # 6 p. 355 - 356
反应条件
N-iodo-succinimide; trifluorormethanesulfonic acid in dichloromethane; water T=20°C; 1 h;
参考文献
Pornsuriyasak, Papapida; Demchenko, Alexei V.
Chemistry - A European Journal, 2006 , vol. 12, # 25 p. 6630 - 6646
反应条件
1: With trifluorormethanesulfonic acid; tetra-n-butylammonium tetrafluoroborate in dichloromethane T=-78°C; Electrochemical reaction; 2: With methanol in dichloromethane T=-78°C;
参考文献
Suzuki, Shinkiti; Matsumoto, Kouichi; Kawamura, Kohsuke; Suga, Seiji; Yoshida, Jun-Ichi
Organic Letters, 2004 , vol. 6, # 21 p. 3755 - 3758
反应条件
I(pyridine)2BF4 in dichloromethane T=23°C; 3 h; Title compound not separated from byproducts.;
参考文献
Huang, Kuo-Ting; Winssinger, Nicolas
European Journal of Organic Chemistry, 2007 , # 12 p. 1887 - 1890
反应条件
trifluorormethanesulfonic acid in dichloromethane T=-35°C; 1 h; Product distribution; Further Variations:Temperaturesreagent ratio;
参考文献
Huang, Kuo-Ting; Winssinger, Nicolas
European Journal of Organic Chemistry, 2007 , # 12 p. 1887 - 1890
反应条件
1: N-bromosuccinimide; water / acetone / 20 °C 2: 1,8-diazabicyclo[5.4.0]undec-7-ene / CH2Cl2 / 0 °C View Scheme
参考文献
Uriel, Clara; Gomez, Ana M.; Lopez, J. Cristobal; Fraser-Reid, Bert
Journal of Carbohydrate Chemistry, 2005 , vol. 24, # 4-6 p. 665 - 675
反应条件
tetra-n-butylammonium tetrafluoroborate; potassium carbonate in acetonitrile Ambient temperatureelectrolyse; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Aloui; Fairbanks
Synlett, 2001 , # 6 p. 797 - 799
反应条件
N-iodo-succinimide; trifluorormethanesulfonic acid in dichloromethane; water T=20°C; 1 h;
参考文献
Pornsuriyasak, Papapida; Demchenko, Alexei V.
Chemistry - A European Journal, 2006 , vol. 12, # 25 p. 6630 - 6646
