反-4-(4-甲氧苯基)-3-丁烯-2-酮合成路线 (共 72 条)
反应条件
1.1: 90 percent / H2 / Pd/C / ethanol / 20 °C / 3102.89 Torr 2.1: LDA / tetrahydrofuran / 0.33 h / -78 °C 2.2: tetrahydrofuran / 3 h / -78 - 20 °C 3.1: 72 percent / 1,4-dicyanonaphthalene / acetonitrile; H2O / 4 h / Irradiation View Scheme
参考文献
Pandey, Ganesh; Karthikeyan; Murugan
Journal of Organic Chemistry, 1998 , vol. 63, # 9 p. 2867 - 2872
反应条件
1-methyl-pyrrolidin-2-one; potassium carbonate; thiophenol 0.5 h; Heating;
参考文献
Chakraborti, Asit K.; Sharma, Lalima; Nayak, Mrinal K.
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6406 - 6414
反应条件
hydrogen; nickel monoaluminide; palladium in diethyl ether; ethyl acetate
参考文献
Eli Lilly and Company
Patent: US3987200 A1, 1976 ;
参考文献
Einhorn; Grabfield
Justus Liebigs Annalen der Chemie, 1888 , vol. 243, p. 370
反应条件
potassium carbonate in ethanol 4 h; Heating;
参考文献
Peseke, Klaus; Goetze, Lutz; Reinke, Helmut; Cedeno, Quirino Arias; Suarez, Jose Quincoces; Andreu, Mario Gomez; Castro, Herman Velez
Journal fur Praktische Chemie - Chemiker - Zeitung, 1997 , vol. 339, # 7 p. 656 - 659
反应条件
hydrogen; palladium on activated charcoal in ethanol T=20°C; Catalytic hydrogenation; P=3102.89 Torr;
参考文献
Pandey, Ganesh; Karthikeyan; Murugan
Journal of Organic Chemistry, 1998 , vol. 63, # 9 p. 2867 - 2872
反应条件
acetone; palladium dichloride Hydrogenation;
参考文献
Li, Xuefeng; Li, Liangchun; Tang, Yuanfu; Zhong, Ling; Cun, Linfeng; Zhu, Jin; Liao, Jian; Deng, Jingen
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 2981 - 2988
反应条件
acetic acid ester; ethanol; water bei der elektrolytischen Reduktion;
参考文献
Law
Journal of the Chemical Society, 1912 , vol. 101, p. 1017
Journal of the Chemical Society, 1912 , vol. 101, p. 1550
反应条件
sodium tetrahydroborate in methanol 0.5 h; Heating;
参考文献
Tetrahedron Asymmetry, , vol. 15, # 2 p. 335 - 340
反应条件
1: ethanol; aq. HCl / 24 h / Ambient temperature View Scheme
参考文献
Dimmock; Smith; Brenner; et al.
European Journal of Medicinal Chemistry, 1986 , vol. 21, # 3 p. 187 - 192