反应条件
1: 11 percent / Me3SiCl, NaI, MeCN, H2O / hexane / 24 h / Ambient temperature
2: 1) LDA, 2) CeCl3 / 1) THF, -78 deg C, 1 h, 2) THF, -78 deg C, 1 h, 3) THF, -78 deg C, 3 h
3: 1) Me3SiCl, NaI, MeCN, 2) K2CO3 / 1) hexane, RT, 24 h, 2) THF, RT, 20 h
View Scheme
参考文献
Sakai; Miyata; Tsuboi; Takeda; Utaka; Torii
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 11 p. 3537 - 3541
