戊烷-2-基4-甲基苯磺酸酯合成路线 （共 10 条）
反应条件
1: acetone; sodium iodide 2: ethanol 3: acetic acid; aqueous hydrogen peroxide 4: ethanolic potassium ethylate View Scheme
参考文献
Brown; Wheeler
Journal of the American Chemical Society, 1956 , vol. 78, p. 2199,2201
反应条件
acetone; sodium iodide
参考文献
Brown; Wheeler
Journal of the American Chemical Society, 1956 , vol. 78, p. 2199,2201
反应条件
1: acetone; sodium iodide 2: ethanolic potassium ethylate / 80 °C View Scheme
参考文献
Brown; Moritani
Journal of the American Chemical Society, 1955 , vol. 77, p. 3607,3609
反应条件
potassium acetate; acetic anhydride; acetic acid
参考文献
Brown; Moritani
Journal of the American Chemical Society, 1955 , vol. 77, p. 3607,3609
反应条件
1: acetone; sodium iodide 2: ethanol View Scheme
参考文献
Brown; Wheeler
Journal of the American Chemical Society, 1956 , vol. 78, p. 2199,2201
反应条件
1: acetone; sodium iodide 2: ethanol 3: acetic acid; aqueous hydrogen peroxide View Scheme
参考文献
Brown; Wheeler
Journal of the American Chemical Society, 1956 , vol. 78, p. 2199,2201
反应条件
sodium bromide; diethylene glycol
参考文献
Brown; Wheeler
Journal of the American Chemical Society, 1956 , vol. 78, p. 2199,2201
反应条件
1.) CuCN 1) THF, -78 deg C, 2) THF, RT, 7 h; Yield given. Multistep reaction;
参考文献
Lipshutz, Bruce H.; Wilhelm, Robert S.; Floyd, David M.
Journal of the American Chemical Society, 1981 , vol. 103, # 25 p. 7672 - 7674
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=0 - 20°C; 4 h; Inert atmosphere;
参考文献
THE JOHNS HOPKINS UNIVERSITY; LIU, Jun, O.; SHI, Wei; PASUNOOTI, Kalyan, Kumar
Patent: WO2013/36866 A1, 2013 ;
Location in patent: Paragraph 0252 ;
反应条件
T=60°C; Rate constantMechanism;
参考文献
Eliel,E.L.; Knox,D.E.
Journal of the American Chemical Society, 1985 , vol. 107, p. 2946
