ethanol; sodium; benzene

1: 97 percent / pyridine, 4-N,N-dimethylaminopyridine / CH2Cl2 / 1.) 0 deg C, 2.) 3 h, room temperature 2: 79.2 percent / NaH / tetrahydrofuran / 10 h / Heating 3: 67 percent / Et4NOTs, HOAc, t-BuOH / Ambient temperature; anodic oxidation (3.3 mA cm-1); var. electrolyte, var. solvent, var. electricity 4: K2CO3 / dimethylformamide / 75 - 80 °C 5: 91.7 percent / 2N aq. NaOH / 3 h / Heating View Scheme

ethanol; sodium; benzene

2: KOH View Scheme

1: KOH View Scheme

sulfuric acid

暂无反应条件数据

1: 97 percent / pyridine, 4-N,N-dimethylaminopyridine / CH2Cl2 / 1.) 0 deg C, 2.) 3 h, room temperature 2: 79.2 percent / NaH / tetrahydrofuran / 10 h / Heating 3: 67 percent / Et4NOTs, HOAc, t-BuOH / Ambient temperature; anodic oxidation (3.3 mA cm-1); var. electrolyte, var. solvent, var. electricity View Scheme