3-苯基环戊-2-烯-1-酮合成路线 （共 62 条）
反应条件
1: 46 percent / aluminium chloride / CCl4 / 0.5 h / 50 °C / Heating
2: 81 percent / basic aluminium oxide / toluene / 3 h / Heating
View Scheme
参考文献
Kjeldsen, Gunhild; Knudsen, Jes S.; Ravn-Petersen, Lise S.; Torssell, Kurt B. G.
Tetrahedron, 1983 , vol. 39, # 13 p. 2237 - 2240
参考文献
Knupp; Hambloch; Frahm
Archiv der Pharmazie, 1985 , vol. 318, # 10 p. 918 - 922
反应条件
1: (i) NaH, (ii) aq. KOH
2: aq. KOH
View Scheme
参考文献
Farnum,D.G. et al.
Journal of Organic Chemistry, 1971 , vol. 36, # 5 p. 698 - 702
反应条件
1: Et3N, 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide / ethanol / 40 h / 65 - 70 °C
2: 1percent aq. NaOH / ethanol / 3.5 h / Heating
View Scheme
参考文献
Nash, Geoffrey; Waring, Anthony John
Journal of Chemical Research, Miniprint, 1988 , # 8 p. 1811 - 1823
反应条件
1: diisopropylamine, butyllithium / tetrahydrofuran / 0.5 h / -80 °C
2: 48 percent / hydrochloric acid, formaldehyde / acetone; H2O / 1 h / Ambient temperature
3: 87 percent / sodium hydride / benzene / Heating
View Scheme
参考文献
Haelters, J. P.; Corbel, B.; Sturtz, G.
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 44, p. 53 - 74
反应条件
1: 48 percent / hydrochloric acid, formaldehyde / acetone; H2O / 1 h / Ambient temperature
2: 87 percent / sodium hydride / benzene / Heating
View Scheme
参考文献
Haelters, J. P.; Corbel, B.; Sturtz, G.
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 44, p. 53 - 74
反应条件
hydrogenchloride
Heating;
参考文献
Kato; Katagiri
Chemical and Pharmaceutical Bulletin, 1973 , vol. 21, # 4 p. 729 - 735
参考文献
Kubota,T. et al.
Bulletin of the Chemical Society of Japan, 1965 , vol. 38, p. 1191 - 1194
反应条件
dipyridine chromium trioxide in dichloromethane
T=0°C; 2 h;
参考文献
Singh, Chandan; Saxena, Gunjan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 11 p. 1176 - 1177
参考文献
Yokoyama,T.; Izui,N.
Bulletin of the Chemical Society of Japan, 1965 , vol. 38, p. 1501 - 1503
