(5E,9E,13E)-6,10,14,18-四甲基十九碳-5,9,13,17-四烯-2-酮合成路线 (共 20 条)
反应条件
1: phosphorus tribromide
2: sodium / ethanol
3: 288 mg
4: lithium aluminium hydride
5: phosphorus tribromide
6: sodium / ethanol
View Scheme
参考文献
Suga, Takayuki; Shishibori, Tsuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2098 - 2104
反应条件
1: 288 mg
2: lithium aluminium hydride
3: phosphorus tribromide
4: sodium / ethanol
View Scheme
参考文献
Suga, Takayuki; Shishibori, Tsuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2098 - 2104
反应条件
1: phosphorus tribromide
2: sodium / ethanol
View Scheme
参考文献
Suga, Takayuki; Shishibori, Tsuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2098 - 2104
反应条件
potassium hydroxide in methanol
参考文献
Vig,O.P. et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1979 , vol. 17B, p. 31 - 33
反应条件
1: sodium / ethanol
2: 131 mg / sodium hydride / 1,2-dimethoxy-ethane / 48 h
3: 1.68 g / lithium aluminium hydride / diethyl ether / 2 h / Heating
4: phosphorus tribromide
5: sodium / ethanol
6: 288 mg
7: lithium aluminium hydride
8: phosphorus tribromide
9: sodium / ethanol
View Scheme
参考文献
Suga, Takayuki; Shishibori, Tsuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2098 - 2104
反应条件
1: 33.6 g / phosphorus tribromide / diethyl ether / 4 h
2: sodium / ethanol
3: 131 mg / sodium hydride / 1,2-dimethoxy-ethane / 48 h
4: 1.68 g / lithium aluminium hydride / diethyl ether / 2 h / Heating
5: phosphorus tribromide
6: sodium / ethanol
7: 288 mg
8: lithium aluminium hydride
9: phosphorus tribromide
10: sodium / ethanol
View Scheme
参考文献
Suga, Takayuki; Shishibori, Tsuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2098 - 2104
反应条件
1: 1.68 g / lithium aluminium hydride / diethyl ether / 2 h / Heating
2: phosphorus tribromide
3: sodium / ethanol
4: 288 mg
5: lithium aluminium hydride
6: phosphorus tribromide
7: sodium / ethanol
View Scheme
参考文献
Suga, Takayuki; Shishibori, Tsuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2098 - 2104
反应条件
1: 131 mg / sodium hydride / 1,2-dimethoxy-ethane / 48 h
2: 1.68 g / lithium aluminium hydride / diethyl ether / 2 h / Heating
3: phosphorus tribromide
4: sodium / ethanol
5: 288 mg
6: lithium aluminium hydride
7: phosphorus tribromide
8: sodium / ethanol
View Scheme
参考文献
Suga, Takayuki; Shishibori, Tsuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2098 - 2104
反应条件
1: sodium / ethanol
2: 288 mg
3: lithium aluminium hydride
4: phosphorus tribromide
5: sodium / ethanol
View Scheme
参考文献
Suga, Takayuki; Shishibori, Tsuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2098 - 2104
反应条件
1: lithium aluminium hydride
2: phosphorus tribromide
3: sodium / ethanol
View Scheme
参考文献
Suga, Takayuki; Shishibori, Tsuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2098 - 2104