(2R)-2-[(8E,10E)-十二碳-8,10-二烯氧基]四氢吡喃合成路线 (共 4 条)
反应条件
methanol; toluene-4-sulfonic acid in water T=60°C;
参考文献
Khrimyan, A. P.; Makaryan, G. M.; Ovanisyan, A. L.; Wimmer, Z.; Romanyuk, M.; et al.
Chemistry of Natural Compounds, 1991 , vol. 27, # 1 p. 103 - 108
Khimiya Prirodnykh Soedinenii, 1991 , # 1 p. 117 - 123
反应条件
toluene-4-sulfonic acid in methanol; water T=60°C; 2 h; Yield given;
参考文献
Popovici, Nicolae
Revue Roumaine de Chimie, 1997 , vol. 42, # 3 p. 221 - 224
反应条件
Multi-step reaction with 3 steps 1: 76 percent / H2SO4 / 15 h / 20 - 60 °C2: 33 percent / H2SO4 / 160 °C / 40 Torr3: Li2CuCl4 / tetrahydrofuran / 3 h / -10 °C
参考文献
Shakova; Zorin; Musavirov; Safarov; Muslukhov; Kharisov; Ishmuratov; Rakhmankulov Chemistry of Natural Compounds, 1996 , vol. 32, # 4 p. 582 - 584
反应条件
Multi-step reaction with 2 steps 1: 33 percent / H2SO4 / 160 °C / 40 Torr2: Li2CuCl4 / tetrahydrofuran / 3 h / -10 °C
参考文献
Shakova; Zorin; Musavirov; Safarov; Muslukhov; Kharisov; Ishmuratov; Rakhmankulov Chemistry of Natural Compounds, 1996 , vol. 32, # 4 p. 582 - 584