5,5,6,6,7,7,8,8,8-九氟辛烷-1-醇合成路线 （共 8 条）
反应条件
in ethanol T=70°C; Tosylation; 1 h;
参考文献
Mureau, Natacha; Guittard, Frederic; Geribaldi, Serge
Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2885 - 2889
反应条件
lithium aluminium tetrahydride
参考文献
DAIKIN INDUSTRIES, LTD
Patent: JP2005/330224 A, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
1: With sodium dithionite; sodium hydrogencarbonate in water; acetonitrile
2: With hydrogenchloride
参考文献
3M INNOVATIVE PROPERTIES COMPANY
Patent: WO2003/102003 A1, 2003 ;
Location in patent: Page 9 ;
反应条件
lithium aluminium tetrahydride in diethyl ether
T=40°C; Reduction; 12 h;
参考文献
Mureau, Natacha; Guittard, Frederic; Geribaldi, Serge
Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2885 - 2889
反应条件
1: K2CO3 / tetrahydrofuran / 24 h / 70 °C
2: KOH / ethanol / 80 °C
3: 3 h / 195 °C
4: LiAlH4 / diethyl ether / 12 h / 40 °C
View Scheme
参考文献
Mureau, Natacha; Guittard, Frederic; Geribaldi, Serge
Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2885 - 2889
反应条件
1: 3 h / 195 °C
2: LiAlH4 / diethyl ether / 12 h / 40 °C
View Scheme
参考文献
Mureau, Natacha; Guittard, Frederic; Geribaldi, Serge
Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2885 - 2889
反应条件
1: KOH / ethanol / 80 °C
2: 3 h / 195 °C
3: LiAlH4 / diethyl ether / 12 h / 40 °C
View Scheme
参考文献
Mureau, Natacha; Guittard, Frederic; Geribaldi, Serge
Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2885 - 2889
反应条件
phosphorus tribromide in diethyl ether
T=40°C; Bromination; 12 h;
参考文献
3M INNOVATIVE PROPERTIES COMPANY
Patent: WO2003/102003 A1, 2003 ;
Location in patent: Page 10 ;
