Alpha-(三氟甲基)二苯甲醇合成路线 （共 40 条）
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 24 h;
参考文献
Jablonski, Lukas; Joubert, Jerome; Billard, Thierry; Langlois, Bernard R.
Synlett, 2003 , # 2 p. 230 - 232
反应条件
1: 2,2,2-trifluoroethane-1,1-diol With potassium tert-butylate in N,N-dimethyl-formamide T=-50°C; 0.583333 h; 2: benzophenone in N,N-dimethyl-formamide T=-50°C; 1 h;
参考文献
Surya Prakash; Zhang, Zhe; Wang, Fang; Munoz, Socrates; Olah, George A.
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3300 - 3305
反应条件
tetramethyl-ammonium fluoride; N,N-dimethyl-formamide in tetrahydrofuran T=-10 - 20°C; 6 h;
参考文献
Large; Roques; Langlois
Journal of Organic Chemistry, 2000 , vol. 65, # 26 p. 8848 - 8856
反应条件
potassium tert-butylate in tetrahydrofuran T=0°C; 1 h;
参考文献
Inschauspe, David; Sortais, Jean-Baptiste; Billard, Thierry; Langlois, Bernard R.
Synlett, 2003 , # 2 p. 233 - 235
反应条件
1: CsF / 1,2-dimethoxy-ethane / 5 h / 80 °C 2: tetrabutylammonium fluoride / tetrahydrofuran / 1 h View Scheme
参考文献
Ahvazi, Behzad C.; Crestini, Claudia; Argyropoulos, Dimitris S.
Journal of Agricultural and Food Chemistry, 1999 , vol. 47, # 1 p. 190 - 201
反应条件
KOC(CH3)3 in tetrahydrofuran chromy.;
参考文献
Buergler, Jonas F.; Togni, Antonio
Chemical Communications, 2011 , vol. 47, # 6 p. 1896 - 1898
反应条件
tetrakis(dimethylamino)ethylene in N,N-dimethyl-formamide T=-20 - 20°C; 8.16667 h; Irradiation;
参考文献
Ait-Mohand, Samia; Takechi, Naoto; Medebielle, Maurice; Dolbier Jr., William R.
Organic Letters, 2001 , vol. 3, # 26 p. 4271 - 4273
反应条件
in diethyl ether T=-80 - 20°C; 2 h;
参考文献
Yamazaki, Takashi; Terajima, Tsukasa; Kawasaki-Taskasuka, Tomoko
Tetrahedron, 2008 , vol. 64, # 10 p. 2419 - 2424
反应条件
potassium tert-butylate in tetrahydrofuran T=25°C; 24 h;
参考文献
Billard, Thierry; Langlois, Bernard R.; Blond, Gaelle
European Journal of Organic Chemistry, 2001 , # 8 p. 1467 - 1471
反应条件
cesium fluoride in tetrahydrofuran 20 h; Heating;
参考文献
Motherwell, William B.; Storey, Lynda J.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 4 p. 491 - 498
