2-氯-1,4-二溴-1,1,2-三氟丁烷合成路线 （共 6 条）
反应条件
hydrazine hydrate; anhydrous copper acetate in isopropyl alcohol T=30°C; P=22800 Torr; 4 h;
参考文献
Igumnov, Sergei M.; Don, Veronika L.; Vyazkov, Vladimir A.; Narinyan, Karen E.
Mendeleev Communications, 2006 , # 3 p. 189 - 190
反应条件
pyridine; phosphorus tribromide in benzene T=20°C; 48 h;
参考文献
Shellhamer, Dale F.; Davenport, Kevyn J.; Forberg, Heidi K.; Herrick, Matthew P.; Jones, Rachel N.; Rodriguez, Sean J.; Sanabria, Sunamita; Trager, Nicole N.; Weiss, Ryan J.; Heasley, Victor L.; Boatz, Jerry A.
Journal of Organic Chemistry, 2008 , vol. 73, # 12 p. 4532 - 4538
反应条件
1: With bromine chloride in dichloromethane T=25°C; 0.333333 h; 2: With [14C]-Tetramethylammonium bromide in dimethyl sulfoxide T=25°C; 96 h; Further stages.;
参考文献
Shellhamer, Dale F.; Davenport, Kevyn J.; Forberg, Heidi K.; Herrick, Matthew P.; Jones, Rachel N.; Rodriguez, Sean J.; Sanabria, Sunamita; Trager, Nicole N.; Weiss, Ryan J.; Heasley, Victor L.; Boatz, Jerry A.
Journal of Organic Chemistry, 2008 , vol. 73, # 12 p. 4532 - 4538
反应条件
bromine chloride in dichloromethane T=25°C; 15 h; Further byproducts.;
参考文献
Shellhamer, Dale F.; Davenport, Kevyn J.; Forberg, Heidi K.; Herrick, Matthew P.; Jones, Rachel N.; Rodriguez, Sean J.; Sanabria, Sunamita; Trager, Nicole N.; Weiss, Ryan J.; Heasley, Victor L.; Boatz, Jerry A.
Journal of Organic Chemistry, 2008 , vol. 73, # 12 p. 4532 - 4538
参考文献
Tarrant; Lilyquist
Journal of the American Chemical Society, 1955 , vol. 77, p. 3640
参考文献
Tarrant; Lilyquist
Journal of the American Chemical Society, 1955 , vol. 77, p. 3640
