1-溴-2-(溴甲基)萘合成路线 (共 51 条)
反应条件
N-bromosuccinmide; meta-chloroperoxybenzoic acid in tetrachloromethane 3 h; Heating;
参考文献
Billups, W. E.; Reed, Larry E.; Casserly, Edward W.; Lin, L. P.
Journal of Organic Chemistry, 1981 , vol. 46, # 7 p. 1326 - 1333
反应条件
dibenzoyl peroxide in tetrachloromethane 3 h; Reflux;
参考文献
Sudheendran, Kavitha; Malakar, Chandi C.; Conrad, Juergen; Beifuss, Uwe
Journal of Organic Chemistry, 2012 , vol. 77, # 22 p. 10194 - 10210
反应条件
1: 91 percent / Br2 / CS2 2: 79 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 3 h / Heating; Irradiation View Scheme
参考文献
Newman; Kosak
Journal of Organic Chemistry, 1949 , vol. 14, p. 375,378
反应条件
bromine; anhydrous lanthanum acetate in tetrachloromethane T=60°C; Irradiation;
参考文献
Ouertani, Mohsen; Girard, Pierre; Kagan, Henry B.
Bulletin de la Societe Chimique de France, 1982 , vol. <2> 2, # 9-10 p. 327 - 328
反应条件
bromine; anhydrous lanthanum acetate in n-heptane T=60 - 62°C; 5.5 h; illuminating with visible light; Yields of byproduct given;
参考文献
Waykole, Liladhar; Prashad, Mahavir; Palermo, Stephen; Repic, Oljan; Blacklock, Thomas J.
Synthetic Communications, 1997 , vol. 27, # 12 p. 2159 - 2163
反应条件
T=230°C; bei der Bromierung im Licht einer Bogenlampe;
参考文献
Mayer,F.; Sieglitz
Chemische Berichte, 1922 , vol. 55, p. 1854
参考文献
Newman; Kosak
Journal of Organic Chemistry, 1949 , vol. 14, p. 375,378
参考文献
Shoesmith; Rubli
Journal of the Chemical Society, 1927 , p. 3104
Full Text Show Details
Mayer,F.; Sieglitz
Chemische Berichte, 1922 , vol. 55, p. 1854
参考文献
Shoesmith; Rubli
Journal of the Chemical Society, 1927 , p. 3104
Full Text Show Details
Mayer,F.; Sieglitz
Chemische Berichte, 1922 , vol. 55, p. 1854
反应条件
in ethanol T=20°C; 18 h;
参考文献
GENENTECH, INC.
Patent: WO2006/69063 A1, 2006 ;
Location in patent: Page/Page column 62 ;
WO 2006/069063 A1