2,4,6-三甲氧基苯甲酮合成路线 （共 31 条）
反应条件
1: methanol; diethyl ether
2: CCl4; CHCl3 / Ozonolyse
3: aqueous KOH
View Scheme
参考文献
Polonsky
Bulletin de la Societe Chimique de France, 1955 , p. 541,543
反应条件
1: CCl4; CHCl3 / Ozonolyse
2: aqueous KOH
View Scheme
参考文献
Polonsky
Bulletin de la Societe Chimique de France, 1955 , p. 541,543
参考文献
Polonsky
Bulletin de la Societe Chimique de France, 1955 , p. 541,543
反应条件
in diethyl ether
-78 deg C to r.t.;
参考文献
Nagel, Ulrich; Nedden, Hans Guenter
Chemische Berichte, 1997 , vol. 130, # 7 p. 989 - 1006
参考文献
Ciamician; Silber
Chemische Berichte, 1891 , vol. 24, p. 300
Chemische Berichte, 1892 , vol. 25, p. 1120
参考文献
Spaeth; Fuchs
Monatshefte fuer Chemie, 1921 , vol. 42, p. 272
参考文献
Ciamician; Silber
Chemische Berichte, 1894 , vol. 27, p. 1497,1499
反应条件
1: With boron tribromide in dichloromethane
T=-78 - 20°C; 48 h; Inert atmosphere;
2: With water in dichloromethane
T=0 - 20°C; 1.3 h;
参考文献
Thevenin, Marion; Mouray, Elisabeth; Grellier, Philippe; Dubois, Joelle
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2986 - 2992
反应条件
N-ethyl-N,N-diisopropylamine in toluene
T=100°C; 16 h;
参考文献
Brajeul, Solenn; Delpech, Bernard; Marazano, Christian
Tetrahedron Letters, 2007 , vol. 48, # 32 p. 5597 - 5600
参考文献
Jobst; Hesse
Justus Liebigs Annalen der Chemie, 1879 , vol. 199, p. 73
