in tetrahydrofuran
reaction at -30 - 25°C, later at 50°C, several hours and dehydration of the dihydroxide over P2O5;;
参考文献
Pierce; Levine
Journal of the American Chemical Society, 1953 , vol. 75, p. 1254
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
Kurykin, M. A.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 11 p. 2389
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 11 p. 2649
in further solvent(s)
reaction in n-butyl ether at -20°C, 3 hours, stirring for 24 hours, warming to 20°C within 12 - 15 hours and heating to 50°C, 0.5 hours;;
in further solvent(s)
addition of the grignard compound to the ester in n-butyl ether at -50°C, stirring at -40°C, 24 hours, warming to 20°C within 24 hours and stirring for 24 hours;;
