1-(2-(3-甲氧基苯基)乙炔)苯合成路线 （共 27 条）
反应条件
potassium acetate; palladium diacetate; silver(l) oxide in dichloromethane
T=20°C; 12 h; Molecular sieve;
参考文献
Feng, Chao; Loh, Teck-Peng
Chemical Communications, 2010 , vol. 46, # 26 p. 4779 - 4781
反应条件
diisopropyl-carbodiimide in dichloromethane
T=25°C; 24 h; Inert atmosphere;
参考文献
Wardrop, Duncan J.; Komenda, John P.
Organic Letters, 2012 , vol. 14, # 6 p. 1548 - 1551
反应条件
formic acid; 5-hydro-3-oxaoctafluoropentanesulfonyl fluoride; triethylamine; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=80°C; 17 h;
参考文献
Chen, Qing-Yun; He, Ya-Bo
Synthesis, 1988 , # 11 p. 896 - 897
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran; pentane
T=25°C; 3 h; Inert atmosphere;
参考文献
Truong, Thanh; Daugulis, Olafs
Organic Letters, 2011 , vol. 13, # 16 p. 4172 - 4175
反应条件
tris(dibenzylideneacetone)dipalladium (0); N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide
T=80°C; Stille reaction; 10 h;
参考文献
Shen, Wang; Wang, Le
Journal of Organic Chemistry, 1999 , vol. 64, # 24 p. 8873 - 8879
反应条件
copper(l) iodide; cesium fluoride in toluene; acetonitrile
T=150°C; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Akubathini, Shashidhar Kumar; Biehl, Ed
Tetrahedron Letters, 2009 , vol. 50, # 16 p. 1809 - 1811
反应条件
tert.-butylnitrite; trifuran-2-yl-phosphane; palladium diacetate; acetic acid in dimethyl sulfoxide
T=20 - 32°C; Sonogashira coupling; 16 h; Inert atmosphere;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Chemical Communications, 2011 , vol. 47, # 28 p. 7959 - 7961
反应条件
copper(l) iodide; 8-hydroxy-quinoline; potassium carbonate in N,N-dimethyl-formamide
T=110°C; 24 h; Inert atmosphere;
参考文献
Yan, Hong; Lu, Linhua; Sun, Peng; Zhu, Yan; Yang, Hailong; Liu, Defu; Rong, Guangwei; Mao, Jincheng
RSC Advances, 2013 , vol. 3, # 2 p. 377 - 381
反应条件
potassium phosphate; bis(η3-allyl-μ-chloropalladium(II)); N,N,N′,N′-tetra(diphenylphosphinomethyl)pyridine-2,6-diamine in N,N-dimethyl acetamide; water
T=100°C; Sonogashira Cross-Coupling; 6 h; Schlenk techniqueInert atmosphere;
参考文献
Zhou, Rong; Wang, Wei; Jiang, Zhi-Jie; Fu, Hai-Yan; Zheng, Xue-Li; Zhang, Chun-Chun; Chen, Hua; Li, Rui-Xiang
Catalysis Science and Technology, 2014 , vol. 4, # 3 p. 746 - 751
反应条件
palladium diacetate; triethylamine; triphenylphosphine in N,N-dimethyl acetamide
T=100°C; 3 h;
参考文献
Mataka; Liu; Tashiro
Synthesis, 1995 , # 2 p. 133 - 135
