1,1,1-三甲基-N-苯基哌啶合成路线 （共 76 条）
反应条件
nitrosyl chloride in dichloromethane
0.166667 h; Ambient temperature;
参考文献
Weiss, Robert; Wagner, Klaus-Georg; Hertel, Marion
Chemische Berichte, 1984 , vol. 117, # 5 p. 1965 - 1972
反应条件
hydrogenchloride; n-butyllithium
1.) THF, hexane, 0 deg C, 0.5 h, 2.) ether, 0 deg C; Yield given. Multistep reaction;
参考文献
Calverley, Martin J.
Synthetic Communications, 1983 , vol. 13, # 7 p. 601 - 610
反应条件
lithium perchlorate in diethyl ether
0.5 h;
参考文献
Saidi, Mohammad R; Azizi, Najmoddin; Zali-Boinee, Hasan
Tetrahedron, 2001 , vol. 57, # 31 p. 6829 - 6832
反应条件
nitrosyl bromide in dichloromethane
0.166667 h; Ambient temperature;
参考文献
Weiss, Robert; Wagner, Klaus-Georg; Hertel, Marion
Chemische Berichte, 1984 , vol. 117, # 5 p. 1965 - 1972
反应条件
in benzene
T=0°C; 1 h;
参考文献
Schmidt, Arthur H.; Debo, Michael; Wehner, Bernhard
Synthesis, 1990 , # 3 p. 237 - 242
反应条件
lithium perchlorate in diethyl ether
0.5 h;
参考文献
Saidi, Mohammad R; Azizi, Najmoddin; Zali-Boinee, Hasan
Tetrahedron, 2001 , vol. 57, # 31 p. 6829 - 6832
反应条件
tetrabutyl ammonium fluoride in N,N-dimethyl-formamide
T=20°C; 0.0833333 h;
参考文献
Iida, Akira; Horii, Atsushi; Misaki, Tomonori; Tanabe, Yoo
Synthesis, 2005 , # 16 art. no. F06305SS, p. 2677 - 2682
反应条件
N-bromosuccinmide in tetrachloromethane
T=-20°C; 24 h;
参考文献
Ando, Wataru; Tsumaki, Hidetoshi
Synthesis, 1982 , # 4 p. 263 - 264
反应条件
1: PI5 / benzene
2: NaOMe / methanol
View Scheme
参考文献
Kostina,V.G.; Feshchenko,N.G.
J. Gen. Chem. USSR (Engl. Transl.), 1979 , vol. 49, # 11 p. 2452 - 2458,2165 - 2169
反应条件
methyl iodide in hexane
20 h; Heating;
参考文献
Hamada, Yoshitaka; Yamamoto, Yasushi; Shimizu, Hideaki
Journal of Organometallic Chemistry, 1996 , vol. 510, # 1-2 p. 1 - 6
